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Method for preparing printing paste from corn starch

A technology for printing paste and corn starch, which is applied in the field of printing paste preparation, can solve the problems of affecting the quality of fabrics, reducing the paste formation rate, poor penetration effect, etc., and achieves the effects of improving paste formation effect, low cost and high penetration rate

Inactive Publication Date: 2017-03-15
CHANGZHOU YAHUAN ENVIRONMENTAL PROTECTION TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The technical problem to be solved by the present invention: in view of the poor penetration effect of the existing printing paste, which reduces its paste rate, affects the quality of the fabric, and causes its poor hand feeling, the present invention first uses hydrogen peroxide to oxidize corn starch treatment, followed by aloe vera gel to adjust the viscosity, modified by microorganisms, supplemented with ammonium carbonate to increase its permeability, then added 3-chloro-2-hydroxypropyltrimethylammonium chloride for etherification treatment, and finally mixed with cinnamon acid to react to prepare printing paste, the printing paste prepared by the present invention has good permeability, improves its paste rate, and makes the fabric feel soft after use

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0017] First, according to the mass ratio of 1:3, take cornstarch and 15% hydrogen peroxide in a mass fraction and put them into a three-necked flask with a thermometer and a stirrer, use oxygen protection, and move the three-necked flask to a water bath, set the temperature to 90 ℃, stirred at 150r / min for 3h, then naturally cooled to room temperature, vacuum-filtered the mixture in the three-necked flask, and collected the filter residue; then, in parts by weight, took 50 parts of filter residue, 16 parts of aloe vera gel, and 7 parts of tetrasporum Mushrooms, 6 parts of deionized water and 2 parts of ammonium carbonate were put into a blender, stirred evenly and put into a container, keeping the temperature in the container at 26°C, stirring at 100r / min for 2h, then stopping the stirring, sealing the container, and using nitrogen gas Discharge the air in the container and let it stand for 50 minutes; after the above standing, add distilled water twice the mass of the mixture...

example 2

[0020] First, according to the mass ratio of 1:3, put cornstarch and 15% hydrogen peroxide into a three-necked flask with a thermometer and a stirrer, use oxygen protection, and move the three-necked flask to a water bath, set the temperature to 80 ℃, stirred at 150r / min for 2h, then naturally cooled to room temperature, and vacuum-filtered the mixture in the three-neck flask to collect the filter residue; then, in parts by weight, take 40 parts of filter residue, 13 parts of aloe vera gel, and 5 parts of tetrasporum Mushrooms, 3 parts of deionized water and 1 part of ammonium carbonate were put into a blender, stirred evenly, then put into a container, kept the temperature in the container at 24°C, stirred at 100r / min for 1 hour, then stopped stirring, sealed the container, and used nitrogen gas Discharge the air in the container and let it stand for 40 minutes; after the above-mentioned standing, add distilled water of 1 times the mass of the mixture in the container to the c...

example 3

[0023]First, according to the mass ratio of 1:3, take cornstarch and 15% hydrogen peroxide into a three-necked flask with a thermometer and a stirrer, use oxygen protection, and move the three-necked flask to a water bath, set the temperature to 85 ℃, stirred at 150r / min for 2h, then naturally cooled to room temperature, and vacuum-filtered the mixture in the three-necked flask to collect the filter residue; then, in parts by weight, take 45 parts of filter residue, 15 parts of aloe vera gel, and 6 parts of tetrasporum Mushrooms, 4 parts of deionized water and 1 part of ammonium carbonate were put into a blender, stirred evenly and put into a container, keeping the temperature in the container at 25°C, stirring at 100r / min for 1 hour, then stopping the stirring, sealing the container, and using nitrogen gas Discharge the air in the container and let it stand for 45 minutes; after the above-mentioned standing, add distilled water of 1 times the mass of the mixture in the contain...

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Abstract

The invention relates to a method for preparing printing paste from corn starch, and belongs to the technical field of printing paste preparation. The method comprises the steps that oxidation treatment is firstly conducted on the corn starch through hydrogen peroxide, the viscosity is regulated with aloe gel, modification is conducted through microorganisms, the permeability of the corn starch is improved through assistance of ammonium carbonate, and then 3-chloro-2-hydroxypropyltrimethylammonium chloride is added for etherification treatment; finally, the corn starch reacts with cinnamic acid, and then the printing paste is prepared. According to the printing paste prepared through the method, the permeability is high and reaches 35% or above, the paste forming effect is improved, and the paste forming rate reaches 7.8%-13.5%; after the printing paste is used, a fabric is uniform in obtained color, high in color fastness and soft and smooth in handfeel.

Description

technical field [0001] The invention relates to a method for preparing printing paste based on cornstarch, and belongs to the technical field of printing paste preparation. Background technique [0002] Printing paste refers to a polymer compound that can thicken the printing paste. Before the printing paste is added to the printing paste, it is generally soluble in water, or a hydrophilic polymer thick colloid solution that can fully swell and disperse in water, or an oil / water type or water / oil type emulsified paste . When preparing printing paste, part of the dye is dissolved in water, and the other part is dissolved, adsorbed or dispersed in the original printing paste. Printing paste is the main component of printing paste. As the carrier and medium of dyes and auxiliaries in the printing process, it determines the running performance of printing, the amount of color given by dyes, the smoothness and clarity of pattern outlines, etc. In short, the quality of printing...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08B31/16C08B31/18D06P1/48
CPCC08B31/16C08B31/185D06P1/48
Inventor 高玉梅薛荣飞邹玉
Owner CHANGZHOU YAHUAN ENVIRONMENTAL PROTECTION TECH
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