Preparation method of silicon carbon microcrystalline composite material for dynamic seal of internal combustion engine
A composite material, silicon carbon technology, applied in the direction of lubricating composition, petroleum industry, additives, etc., to achieve the effect of good lubrication and sealing performance
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[0019] The invention provides a method for preparing a silicon-carbon microcrystalline composite material used for internal combustion engine sealing, comprising:
[0020] Step 1, placing polysilicon and graphite powder in a ball mill, and ball milling to obtain a silicon-carbon mixture with a particle size of less than 15 μm;
[0021] Step 2. Put the silicon-carbon mixture in the induction furnace, firstly carry out vacuum treatment, so that the absolute pressure in the induction furnace reaches 0.0.001Pa, and then fill the induction furnace with argon gas, first make the induction furnace The absolute pressure in the furnace is raised to 0.01MPa, and maintained at this pressure for 10-15 minutes, and then continue to feed argon, so that the absolute pressure in the induction furnace is raised to 0.03MPa, and maintained at this pressure for 5-7min , and then continue to feed argon, so that the absolute pressure in the induction furnace rises to 0.05MPa, and maintain the press...
Embodiment 1
[0030] Step 1, placing polysilicon and graphite powder in a ball mill, and ball milling to obtain a silicon-carbon mixture with a particle size of less than 15 μm;
[0031] Step 2. Put the silicon-carbon mixture in the induction furnace, firstly carry out vacuum treatment, so that the absolute pressure in the induction furnace reaches 0.0.001Pa, and then fill the induction furnace with argon gas, first make the induction furnace The absolute pressure in the furnace was raised to 0.01MPa, and maintained at this pressure for 15 minutes, then continued to feed argon, so that the absolute pressure in the induction furnace was raised to 0.03 MPa, and maintained at this pressure for 7 minutes, and then continued to pass through Enter argon to raise the absolute pressure in the induction furnace to 0.05 MPa, and maintain the pressure for 3 minutes; then start heating, raise the temperature in the induction furnace to 1400 ° C, and continue heating at this temperature for 15 minutes ;...
Embodiment 2
[0035] Step 1, placing polysilicon and graphite powder in a ball mill, and ball milling to obtain a silicon-carbon mixture with a particle size of less than 15 μm;
[0036] Step 2. Put the silicon-carbon mixture in the induction furnace, firstly carry out vacuum treatment, so that the absolute pressure in the induction furnace reaches 0.0.001Pa, and then fill the induction furnace with argon gas, first make the induction furnace The absolute pressure in the furnace rose to 0.01MPa, and maintained at this pressure for 10 minutes, then continued to feed argon, so that the absolute pressure in the induction furnace rose to 0.03MPa, and maintained at this pressure for 5 minutes, and then continued to pass through Enter argon to raise the absolute pressure in the induction furnace to 0.05 MPa, and maintain the pressure for 2 minutes; then start heating, raise the temperature in the induction furnace to 1400 ° C, and continue heating at this temperature for 10 minutes ; Then stop he...
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