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Multiple composite gel leak-stopping agent used for well drilling

A technology of composite gel and plugging agent, which is applied in the directions of drilling compositions, chemical instruments and methods, etc., can solve the problems of easy softening and corrosion of the plugging agent, failure of plugging, and high cost.

Inactive Publication Date: 2017-05-03
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, CN103911133A discloses a plugging composition containing fruit shells, sawdust, mica, and straw, which achieves effective plugging through different particle sizes; LCM and kelp powder, etc. Although these materials can improve the plugging effect to a certain extent, the wells are usually under extreme conditions of high temperature, high pressure and corrosion. The above-mentioned plugging materials or plugging agents are easy to change. Soft corrosion, resulting in plugging failure or secondary leakage
CN104531109A, CN104498000A, CN102443383A, etc. disclose composite plugging agents made of new chemical materials, but these often cause relatively large environmental pollution, and the cost is high, and are not suitable for a large amount of use in drilling plugging
CN104559973A discloses an elastic plugging agent, which is mainly composed of elastic temporary plugging particles and a bridging agent, which can expand to form a plugging layer when exposed to water, but the time for forming the plugging layer cannot be adjusted

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] This embodiment provides a multi-component composite gel plugging agent, which includes components in parts by weight:

[0024] 5 parts by weight of rigid walnut shell particles (40% of the particle size is distributed in the 40~60 mesh walnut shell particles, 60% of the particle size is distributed in the 60~100 mesh walnut shell particles), 15 parts by weight of the flexible material asbestos fiber (the diameter is 0.001~0.5mm , length 1~3mm), 80 parts by weight of polyacrylamide as a solidifying polymer, and 10 parts by weight of accelerator hexamethylenetetramine / phenol (the molar ratio of hexamethylenetetramine to phenol is 3:1).

[0025] The multi-component composite gel plugging agent in this embodiment is obtained by weighing the raw material components of the plugging agent according to the proportion and adding them into a mixer or kneader to mix and stir evenly under normal temperature and pressure conditions.

[0026] Add 4wt% of the multi-component composit...

Embodiment 2

[0028] This embodiment provides a multi-component composite gel plugging agent, which includes components in parts by weight:

[0029] 10 parts by weight of rigid cottonseed hull particles (50% of the particle size distribution is 40~60 mesh cottonseed hull particles, 50% particle size distribution is 60~100 mesh cottonseed hull particles), 10 parts by weight of flexible material polypropylene fiber (diameter 0.001~0.5 mm, length 0.5~2mm), 75 parts by weight of solidified polymer poly(acrylamide-sodium polyacrylate), 5 parts by weight of accelerator hexamethylenetetramine / hydroquinone (hexamethylenetetramine and The molar ratio of hydroquinone is 5:1).

[0030] The multi-component composite gel plugging agent in this embodiment is obtained by weighing the raw material components of the plugging agent according to the proportion and adding them into a mixer or kneader to mix and stir evenly under normal temperature and pressure conditions.

[0031] Add 6wt% of the multi-compon...

Embodiment 3

[0033] This embodiment provides a multi-component composite gel plugging agent, which includes components in parts by weight:

[0034] 8 parts by weight of rigid core sawdust particles (20% particle size distribution is 40~60 mesh sawdust particles, 80% particle size distribution is 60~100 mesh sawdust particles), flexible material polyethylene fiber 10 weight parts (diameter 0.001~0.5mm, 1~3mm in length), 74 parts by weight of polyacrylamide, a solidified polymer, and 8 parts by weight of accelerator hexamethylenetetramine / resorcinol (the molar ratio of hexamethylenetetramine to resorcinol is 8:1).

[0035] The multi-component composite gel plugging agent in this embodiment is obtained by weighing the raw material components of the plugging agent according to the proportion and adding them into a mixer or kneader to mix and stir evenly under normal temperature and pressure conditions.

[0036] Add 5wt% of the multi-component composite gel plugging agent of this embodiment to...

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Abstract

The invention provides a preparation method and application of a multiple composite gel leak-stopping agent. The multiple composite gel leak-stopping agent comprises 5-10 parts by weight of rigid particles, 5-15 parts by weight of a flexible material, 60-85 parts by weight of a curable polymer, and 2-10 parts by weight of an accelerating agent. Components of the leak-stopping agent combine for multiple cooperation. The added rigid particles cooperate with polymer gel to provide bearing capability, and the flexible fiber material improves the tear resistance. Through regulation of the content of the accelerating agent, the curing time of the leak-stopping agent can be controlled to meet different time requirements of the leak-stopping agent for gel forming in the leak conditions with different degrees. The leak-stopping agent can effectively block leak channels, is good in adaptivity, can provide efficient blocking in low or high pressure, and is high in bearing strength. The leak-stopping agent can be used to leak-stopping operation of well drilling, and can overcome the problem of well leak with different degrees and depths.

Description

technical field [0001] The invention relates to the technical field of oil drilling plugging, in particular to a multi-component composite gel plugging agent for drilling. Background technique [0002] Lost circulation is one of the common downhole complex situations in the drilling process. It not only consumes drilling time and loses mud, but also may cause a series of complicated situations such as pipe sticking, blowout, well collapse, etc., and even lead to the scrapping of the wellbore, causing major economic losses. loss. [0003] Lost circulation agent is an indispensable material basis in the process of leak prevention and plugging in drilling engineering, and the use of a good plugging agent is the key to solving the problem of lost circulation. Bridging plugging is generally used in the domestic treatment of lost circulation, which accounts for more than 50% of the entire lost circulation treatment method. Bridging plugging has the advantages of low cost, conveni...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/44
CPCC09K8/44C09K8/426C09K2208/04
Inventor 庞雨微袁俊秀朱魁逯贵广
Owner CHINA PETROLEUM & CHEM CORP