Preparation method of 1-peroxytertbutyl-3-(triethoxysilyl)propane
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A technology of triethoxysilyl and tert-butyl peroxy, which is applied in the field of organic compound synthesis to achieve the effect of increasing the degree of organicization and improving compatibility
Inactive Publication Date: 2017-05-10
QIQIHAR UNIVERSITY
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Problems solved by technology
However, compared with the existing functional organic compounds, most of the structures have only one or a type of special functional group, which can only play a role in one function.
Method used
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Embodiment 1
[0036] Made from raw materials with the following weight ratio components:
[0037] tert-butyl hydroperoxide 3g
[0038] n-Hexane 5g
[0039] Anhydrous Magnesium Sulfate 3g
[0040] 3-Chloropropyltriethoxysilane 8g
[0041] Anhydrous toluene 15ml
[0042] Ferric chloride 0.08g
[0043] Methanol 45ml
[0044] Sodium hydroxide solution 200ml.
Embodiment 2
[0046] Made from raw materials with the following weight ratio components:
[0047] tert-butyl hydroperoxide 5g
[0048] n-Hexane 5g
[0049] Anhydrous Magnesium Sulfate 3g
[0050] 3-Chloropropyltriethoxysilane 8g
[0051] Anhydrous toluene 15ml
[0052] Ferric chloride 0.12g
[0053] Methanol 45ml
[0054] Sodium hydroxide solution 200ml.
Embodiment 3
[0056] Made from raw materials with the following weight ratio components:
[0057] tert-butyl hydroperoxide 8g
[0058] n-Hexane 5g
[0059] Anhydrous Magnesium Sulfate 3g
[0060] 3-Chloropropyltriethoxysilane 8g
[0061] Anhydrous toluene 15ml
[0062] Ferric chloride 0.16g
[0063] Methanol 45ml
[0064] Sodium hydroxide solution 200ml.
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Abstract
The invention discloses a preparation method of 1-peroxytertbutyl-3-(triethoxysilyl)propane and belongs to the technical field of synthesis of organic compounds. According to the method provided by the invention, a molecular structure of a compound can have two functional groups with different functions, wherein peroxy groups of peroxytertbutyl can be decomposed to generate free radicals, so that free radical polymerization is initiated; furthermore, a plurality of ethoxy radicals in triethoxysilyl can be hydrolyzed with inorganic particles with hydroxyl on the surfaces, including TiO2 and the like, and are used for inorganic particle surface modification, so that aspects which cannot be realized by an existing functional organic compound are realized. The 1-peroxytertbutyl-3-(triethoxysilyl)propane is prepared from the following raw materials according to weight ratios: 3g to 8g of tertbutyl hydroperoxide, 5g of n-hexane, 3g of anhydrous magnesium sulfate, 8g of 3-chloropropyltriethoxysilane, 15ml of anhydrous toluene, 0.08g to 0.16g of ferric trichloride, 45ml of methanol and 200ml of a sodium hydroxide solution.
Description
technical field [0001] The invention relates to a preparation method of 1-tert-butylperoxy-3-(triethoxysilyl)propane, which belongs to the technical field of organic compound synthesis. Background technique [0002] Functional organic compounds are a general term for a class of organic compounds with one or more functional groups with special functions in their molecular structures. The synthesis of functional organic compounds mainly covers five aspects: synthetic organic chemistry, bioorganic chemistry, physical organic chemistry, natural organic chemistry, and organic materials. Among them, organic materials are based on the advantages of organic chemistry, and new organic materials, organic-inorganic composites are developed. Materials, design, synthesis and performance research of nanomaterials, expand applications in materials chemistry, nanoscale physical chemistry and other interdisciplinary fields. The research work mainly focuses on the preparation of organic info...
Claims
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Application Information
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