The invention relates to the technical field of
reverse osmosis composite membranes, in particular to a high-temperature-resistant
reverse osmosis membrane prepared based on
acyl chloride graphene oxide and ultrasonic assistance and a preparation method of the high-temperature-resistant
reverse osmosis membrane. According to the preparation method,
acyl chloride and
graphene oxide react to synthesize
acyl chloride graphene oxide (GO-COCl), an isoparaffin
solvent Isopar G serves as a dispersing agent to be added into an organic phase, meanwhile, an organic phase solution is subjected to ultrasonic-assisted treatment before
interfacial polymerization, and GO-COCl is evenly dispersed in the organic phase; and finally, through
interfacial polymerization of m-phenylenediamine (MPD) and 1, 3, 5-tribenzoyl
chloride (TMC), the composite reverse
osmosis membrane is prepared. According to the method, GO-COCl can be added into the PA layer instead of the surface or the substrate through crosslinking, acyl
chloride in GO-COCl reacts with an amine
monomer to form a
polyamide chain, and meanwhile, an organic phase solution is subjected to
ultrasonic dispersion before
interfacial polymerization, so that a uniform GO-COCl sheet is clamped in the PA layer, and the surface of the PA layer is coated with the GO-COCl. The flux, the desalting performance and the stability of the composite reverse
osmosis membrane are favorably improved.