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A kind of preparation method of silicon carbide reinforced aluminum matrix composite material

A technology for composite materials and reinforced aluminum matrix, which is applied in the field of preparation of silicon carbide reinforced aluminum matrix composite materials, can solve the problems of large surface gap between solid phases, easy formation of micro-cracks, and insufficient infiltration of two phases, etc., to achieve improved thermal conductivity , reduce porosity, improve the effect of adhesion

Active Publication Date: 2018-06-29
JIANGXI LEFU IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The wetting and adhesion behavior between the liquid metal and the solid reinforcement phase in the liquid metal method plays a crucial role, and the pores and phase interface states generated between the two phases have a great influence on the mechanical properties, thermophysical properties and Corrosion resistance has a very intuitive impact, but at present, there are few studies on the above-mentioned defects of composite materials manufactured by liquid phase metal method. The phase cannot be fully infiltrated, and material defects such as residual pores and microcracks are easily formed between the two phases, and microcracks are easily formed between the SiC particles and the aluminum matrix, resulting in insufficient performance of the prepared electronic components, which restricts the development of SiCp / Al composite materials.

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  • A kind of preparation method of silicon carbide reinforced aluminum matrix composite material

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Embodiment 1

[0026] A method for preparing a silicon carbide reinforced aluminum-based composite material, the specific steps of which are:

[0027] 1) Preliminary alkali cleaning: first prepare a strong alkali solution with a substance concentration of 2mol / L, then heat the prepared strong alkali solution to 60°C and keep it warm, and immerse the silicon carbide particles in the strong alkali solution for 2 hours. The solution was stirred continuously during the soaking process. After the alkali cleaning is completed, dilute the alkali solution with tap water and filter and separate the silicon carbide particles and the solution, then soak the filtered silicon carbide particles with clean water to remove the remaining alkali solution on the surface of the particles, and then filter and dry to obtain the silicon carbide particles after alkali cleaning .

[0028] 2) Etching: Firstly, a solution with a mass fraction of 4% HF is prepared, and the solution is fully stirred during the preparat...

Embodiment 2

[0034] A method for preparing a silicon carbide reinforced aluminum-based composite material, the specific steps of which are:

[0035] 1) Preliminary alkali cleaning: first prepare a strong alkali solution with a substance concentration of 3mol / L, then heat the prepared strong alkali solution to 70°C and keep it warm, and immerse silicon carbide particles in the strong alkali solution for 3 hours , Stir the solution continuously during the soaking process. After the alkali cleaning is completed, dilute the alkali solution with tap water and filter and separate the silicon carbide particles and the solution, then soak the filtered silicon carbide particles with clean water to remove the remaining alkali solution on the surface of the particles, and then filter and dry to obtain the silicon carbide particles after alkali cleaning .

[0036] 2) Etching: first prepare a solution with a mass fraction of 8% HF, and fully stir the solution during the preparation process so that the...

Embodiment 3

[0042] A method for preparing a silicon carbide reinforced aluminum-based composite material, the specific steps of which are:

[0043] 1) Preliminary alkali cleaning: first prepare a strong alkali solution with a substance concentration of 5mol / L, then heat the prepared strong alkali solution to 80°C and keep it warm, and immerse the silicon carbide particles in the strong alkali solution for 4 hours , Stir the solution continuously during the soaking process. After the alkali cleaning is completed, dilute the alkali solution with tap water and filter and separate the silicon carbide particles and the solution, then soak the filtered silicon carbide particles with clean water to remove the remaining alkali solution on the surface of the particles, and then filter and dry to obtain the silicon carbide particles after alkali cleaning .

[0044] 2) Etching: first prepare a solution with a mass fraction of 10% HF, and fully stir the solution during the preparation process so tha...

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Abstract

The invention discloses a preparation method of an SiC-reinforced aluminum matrix composite. The preparation method comprises the steps of carrying out preliminary alkaline washing to remove Si, SiO2 included slag and an SiO2 film formed on the surface of SiC; carrying out etching on the surface of SiC particles; soaking a precursor solution to obtain SiC particles attached with a precursor phase on the surface; carrying out thermal decomposition to obtain SiC particles attached with an Ir-Cu composite layer on the surface; and carrying out pressureless infiltration to prepare the SiC-reinforced aluminum matrix composite. By using the preparation method of the SiC-reinforced aluminum matrix composite, disclosed by the invention, one Ir-Cu composite layer can be firstly formed on the surface of SiC before pressureless infiltration, the attachment degrees of a reinforced-phase particle interface and an aluminum alloy liquid-phase interface can be effectively improved, and furthermore, holes produced between two phases are reduced, which macroscopically shows that the thermal conductivity of the composite is increased.

Description

technical field [0001] The invention belongs to the field of metal matrix composite materials, in particular to a preparation method of silicon carbide reinforced aluminum matrix composite materials. Background technique [0002] With the rapid development of modern electronic information technology, the internal chip integration of electronic components is rapidly increasing, the power is rapidly increasing, the heat generated by the operation of electronic devices is increasing sharply, and the demand for thermal conductivity of electronic packaging materials is getting higher and higher; at the same time With the improvement of chip integration, the internal structure of electronic products tends to be more complex and refined, which requires higher and higher thermal matching performance of electronic packaging materials and chips and other semiconductor devices. In recent years, the advantages of particle-reinforced metal-matrix composites as electronic packaging materi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C1/10C22C1/02C22C21/00C23C18/08C23C18/04
CPCC22C1/101C22C1/1036C22C21/00C23C18/04C23C18/08
Inventor 周乐平
Owner JIANGXI LEFU IND
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