Process for producing silicon ingots by smelting silicon slag
A silicon ingot and silicon slag technology, applied in the fields of silicon compounds, inorganic chemistry, non-metallic elements, etc., can solve the problems of small capacity, small amount of single smelting, difficulty in mass production, etc.
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Embodiment 1
[0045] A kind of technology that utilizes silicon slag of the present invention to smelt and produce silicon ingot is carried out according to the following steps:
[0046] (a11) Put the silicon block or silicon powder into the intermediate frequency furnace, and add iron block to the intermediate frequency furnace at the same time, the weight of the silicon block and the weight of the iron block are 1:1;
[0047] (a12) Start the intermediate frequency furnace, adjust the operating frequency of the intermediate frequency furnace to 120HZ, the iron block starts to heat up, and the silicon is heated, and the silicon block reaches the melting point and begins to heat up to 1480-1520°C;
[0048] (a13) The silicon block is melted into silicon liquid, and the iron block is taken out, and the furnace is started;
[0049] (b) Silicon smelting: Put the silicon powder into the silicon liquid for smelting. During the silicon smelting process, use a wooden stick to stir the silicon liquid...
Embodiment 2
[0053] A process for producing silicon ingots by smelting silicon slag, comprising the following steps:
[0054] (a21) Put the silicon block or silicon powder into the intermediate frequency furnace, and add aluminum ingots to the intermediate frequency furnace at the same time. The weight of the silicon block and the weight of the aluminum ingot is 2:1;
[0055] (a22) Start the induction furnace, adjust the working frequency of the intermediate frequency furnace to 120HZ, the aluminum ingot starts to heat up, and the temperature rises to 700-800°C, and the aluminum ingot is melted to form aluminum water;
[0056] (a23) Continue to heat up to 1700-1800°C, and melt silicon block or silicon powder into silicon liquid;
[0057] (a24) Increase the silicon content in the silicon-aluminum mixed liquid by gradually adding silicon block or silicon powder to the mixed liquid prepared in step (a23), and pour 85% to 90% of the mixed solution in the induction furnace when it is full The ...
Embodiment 3
[0063] A process for producing silicon ingots by smelting silicon slag, comprising the following steps:
[0064] (a31) Put the silicon block or silicon powder into the intermediate frequency furnace, and add graphite to the intermediate frequency furnace at the same time, the weight of the silicon block and the graphite are 0.6:1;
[0065] (a32) Start the intermediate frequency furnace, adjust the working frequency of the intermediate frequency furnace to 110HZ, the graphite starts to heat up, and the silicon is heated, and the silicon block reaches the melting point and starts to heat up to 1800-1900°C;
[0066] (a33) The silicon block is melted into a silicon liquid, and the graphite is taken out, and the furnace is started;
[0067] (b) Silicon smelting: Put the silicon powder into the silicon liquid for smelting. During the silicon smelting process, use a wooden stick to stir the silicon liquid clockwise or counterclockwise in one direction, and stir 2 to 3 times per minut...
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