Water-washing-resistant natural antibacterial deodorant and preparation method thereof
A natural antibacterial and washable technology, applied in biochemical fiber treatment, textile and papermaking, fiber treatment, etc., to achieve excellent antibacterial effect, good thermal stability and strong adsorption effect
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Embodiment 1
[0028] Dissolve zinc acetate in water, add nano-SiO 2 powder, heated to 75°C, added dropwise absolute ethanol under vigorous stirring, after the dropwise addition, added triammonium citrate, stirred evenly, and stood for 48 hours to prepare a gel, dried the gel, ground it, and Calcined at 480°C for 4h to produce ZnO-SiO 2 composite nanoparticles.
[0029] Prepared ZnO-SiO 2 ZnO and SiO in composite nanoparticles 2 The molar ratio is 3:2.
Embodiment 2
[0031] A preparation method of water-resistant natural antibacterial deodorant, comprising the following steps:
[0032] 1. Add 15 parts of Phellodendron Phellodendron extract, 18 parts of Xihuangcao extract, 30 parts of oregano extract into water and mix evenly, add 20 parts of carboxymethyl chitosan, stir and mix, then mix the ZnO prepared in Example 1 -SiO 2 100 parts of composite nanoparticles were immersed in it, after immersion for 24 hours, dried at 60°C, and then baked at 100°C for 1 hour to prepare loaded nanoparticles;
[0033] 2. Add 100 parts of the loaded nanoparticles prepared in the previous step into the solution in which 20 parts of alginate is dissolved, use a high-shear mixer to stir and disperse at a speed of 10,000 rpm, and then add octadecyl dimethyl beet to it 10 parts of alkali, use ultrasonic instrument to carry out dispersion treatment, make nano-slurry, the solid content of nano-slurry is 60%;
[0034] 3. Mix 100 parts of nano-slurry, 60 parts of w...
Embodiment 3
[0038] A preparation method of water-resistant natural antibacterial deodorant, comprising the following steps:
[0039] 1. Add 20 parts of Phellodendron Phellodendron extract, 25 parts of Xihuangcao extract, 50 parts of oregano extract into water and mix evenly, add 30 parts of carboxymethyl chitosan, stir and mix, then mix the ZnO prepared in Example 1 -SiO 2 100 parts of composite nanoparticles were immersed in it, after immersion for 36 hours, dried at 70°C, and then baked at 120°C for 2 hours to prepare loaded nanoparticles;
[0040] 2. Add 100 parts of the loaded nanoparticles prepared in the previous step into the solution in which 40 parts of alginate is dissolved, use a high-shear mixer to stir and disperse at a speed of 15,000 rpm, and then add octadecyl dimethyl beet to it 17 parts of alkali are dispersed using an ultrasonic instrument to obtain a nano-slurry, and the solid content of the nano-slurry is 70%;
[0041] 3. Mix 100 parts of nano-slurry, 70 parts of wa...
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