A kind of preparation method of mesoporous ceramic
A ceramic and mesoporous technology, which is applied in the field of preparation of mesoporous ceramics, can solve the problems of uneven distribution of pore structure, restricting the comprehensive performance of porous ceramics, and not considering pore-forming agents, so as to improve microporous performance, high-efficiency coating, The effect of high porosity
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[0018] A method for preparing mesoporous ceramics includes the following steps:
[0019] (1) Pore-forming agent modification treatment: Put the starch into an aqueous dopamine hydrochloride solution with 15 times its weight, a temperature of 75°C, and a pH of 8, and stir and mix at 400 rpm for 18 hours, and then increase the speed to 650 rpm / min, slowly add an equal volume of zinc nitrate aqueous solution with a temperature of 65°C and a concentration of 15g / L, stir and react for 45 minutes, and then stand for 3.5 hours, then add 2-methylimidazole equimolar to zinc nitrate, and microwave shaking for 12 hours After suction filtration, the product was washed 3 times with deionized water and then freeze-dried to obtain a pore former coated with an organometallic framework;
[0020] (2) Ingredients: According to the production requirements, the aggregate, the pore former coated with the organometallic framework, and the magnesite are mixed uniformly in a weight ratio of 100:5:0.1, and...
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