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Pt / NH4TiOF3 porous Shaqima-structured photocatalyst and preparation method thereof

A technology of photocatalyst and ammonium fluoride, which is applied in the direction of physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., can solve the problems that the preparation method of porous Sachima structure photocatalyst has not been provided, and achieve dispersion Easy to control, simple process and low preparation cost

Active Publication Date: 2017-08-29
东营睿港投资服务有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Currently, there is no one-step preparation of Pt / NH 4 TiOF 3 Porous Sachima structured photocatalyst and preparation method thereof

Method used

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  • Pt / NH4TiOF3 porous Shaqima-structured photocatalyst and preparation method thereof
  • Pt / NH4TiOF3 porous Shaqima-structured photocatalyst and preparation method thereof
  • Pt / NH4TiOF3 porous Shaqima-structured photocatalyst and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] (1) Get 1ml dipropylene glycol, add 30ml acetic acid successively, 0.4g ammonium fluoride, 0.24g titanium sulfate, 4mg chloroplatinic acid obtain mixed solution;

[0017] (2) Transfer the mixed solution obtained in step (1) to a high-pressure reactor lined with polytetrafluoroethylene, and react at a constant temperature of 180°C for 8 hours;

[0018] (3) Naturally cool the reaction solution obtained in step (2) to room temperature, centrifuge, and repeat washing twice with deionized water and ethanol respectively to obtain Pt / NH 4 TiOF 3 Precipitate;

[0019] (4) Dry the precipitate obtained in step (3) in a 70°C drying oven to obtain Pt / NH 4 TiOF 3 Porous Sachima structured photocatalyst.

Embodiment 2

[0021] (1) Get 1ml dipropylene glycol, add 30ml acetic acid successively, 0.4g ammonium fluoride, 0.24g titanium sulfate, 2mg chloroplatinic acid obtain mixed solution;

[0022] (2) Transfer the mixed solution obtained in step (1) to a high-pressure reactor lined with polytetrafluoroethylene, and react at a constant temperature of 180° C. for 8 hours;

[0023] (3) Naturally cool the reaction solution obtained in step (2) to room temperature, centrifuge, and repeat washing twice with deionized water and ethanol respectively to obtain Pt / NH 4 TiOF 3 Precipitate;

[0024] (4) Dry the precipitate obtained in step (3) in a 70°C drying oven to obtain Pt / NH 4 TiOF 3 Porous Sachima structured photocatalyst.

Embodiment 3

[0026] (1) Get 1ml dipropylene glycol, add 30ml acetic acid successively, 0.4g ammonium fluoride, 0.24g titanium sulfate, 8mg chloroplatinic acid obtain mixed solution;

[0027] (2) Transfer the mixed solution obtained in step (1) to a high-pressure reactor lined with polytetrafluoroethylene, and react at a constant temperature of 180° C. for 8 hours;

[0028] (3) Naturally cool the reaction solution obtained in step (2) to room temperature, centrifuge, and repeat washing twice with deionized water and ethanol respectively to obtain Pt / NH 4 TiOF 3 Precipitate;

[0029] (4) Dry the precipitate obtained in step (3) in a 70°C drying oven to obtain Pt / NH 4 TiOF 3 Porous Sachima structured photocatalyst.

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Abstract

The invention discloses a Pt / NH4TiOF3 porous Shaqima-structured photocatalyst and a preparation method thereof. The Pt / NH4TiOF3 porous Shaqima-structured photocatalyst is characterized in that the Pt / NH4TiOF3 porous Shaqima-structured photocatalyst is prepared by one-step solvothermal reaction. Ammonium fluoride, titanium sulfate and chloroplatinic acid are dissolved in dipropylene glycol and acetic acid to obtain a mixed solution for hydrothermal reaction in a high-pressure reactor with a polytetrafluoroethylene lining, after completion of the reaction, an obtained product is centrifuged, washed and dried to obtain the Pt / NH4TiOF3 porous Shaqima-structured photocatalyst. The method adopts the one-step reaction, and is simple in process and low in preparation cost; the Pt / NH4TiOF3 porous Shaqima-structured photocatalyst prepared by the method has the advantages of high specific surface area and easy-to-control Pt dispersion, and the Pt / NH4TiOF3 porous Shaqima-structured photocatalyst has good photocatalytic activity for hydrogen production by decomposition of water, and has good photocatalytic degradation performance for organic dyes in an aqueous solution.

Description

technical field [0001] The invention belongs to the field of photocatalyst materials and relates to a Pt / NH 4 TiOF 3 Photocatalyst and preparation method thereof, specifically, relate to a kind of Pt / NH 4 TiOF 3 Porous Sachima structured photocatalyst and preparation method thereof. Background technique [0002] Pt is a traditional catalytic material with excellent physical and chemical properties, and has a wide range of applications in electrocatalysis, photocatalysis, solar cells and other fields. However, as a noble metal, Pt resources are scarce and expensive, and problems related to stability and sulfur resistance must be solved urgently. These problems limit the application of noble metal Pt catalysts. Moreover, with the deepening of research, it is found that nano-sized catalyst particles are difficult to operate in practical applications, and due to the small size of nano-catalyst particles, large specific surface area, and thermodynamic instability, they are ea...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J27/24
CPCB01J27/24B01J35/394B01J35/50B01J35/60B01J35/39
Inventor 宋彩霞李洪浩周艳红王德宝赵健
Owner 东营睿港投资服务有限责任公司
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