Axial reactor
A reactor, axial technology, applied in the field of axial reactors, can solve the problems of low production intensity per unit catalyst bed, small bed pressure drop, low heat transfer and mass transfer efficiency, etc., and achieve high target product selectivity. , The effect of improving fluid uniformity and improving the conversion rate of raw materials
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Embodiment 1
[0062] Such as figure 1 As shown, the axial reactor used in this embodiment includes a pressure-bearing shell 2 with an air inlet pipe 18 at the upper end and an air outlet pipe 13 at the lower end. The upper part of the air inlet pipe 18 has an air inlet 1, and the lower part is provided with a first As for the gas distributor 3 , a second gas distributor 17 is arranged below the first gas distributor 3 . There are axial microchannel reaction zone 16 and axial catalytic reaction zone 9 under the intake pipe 18 in the casing 2 , and the axial microchannel reaction zone 16 is arranged directly above the axial catalytic reaction zone 9 . Axial microchannel reaction zone 16 is made of two axial microchannel reaction units 14, comprises bottom sealing plate 15, top sealing plate 4 and sidewall, and its sidewall can overlap with the part sidewall of casing 2, also can be with The side walls of the housing 2 are hermetically connected. The bottom of the housing 2 has a ceramic bal...
Embodiment 2
[0070] Such as Figure 4 , Figure 5 As shown, the reactor of this embodiment is the same as the reactor shell inner diameter of the embodiment 1, the structural parameters such as the axial catalytic reaction zone and the height of the axial microchannel reaction unit are the same. The difference from Example 1 is that in this embodiment, the two axial microchannel reaction units are inverted, that is, the smaller end of the microchannel inlet diameter in this embodiment is the microchannel reaction gas inlet, and the larger diameter end is the product. export port.
[0071] The axial reactor can be used for methanol to olefins reaction.
Embodiment 3
[0073] Such as Image 6 , Figure 7 As shown, the reactor of this embodiment is the same as the reactor shell inner diameter of the embodiment 1, the structural parameters such as the axial catalytic reaction zone and the height of the axial microchannel reaction unit are the same. The difference from Example 1 is that in this example, the axial microchannel reaction zone only includes one axial microchannel reaction unit.
[0074] The reactor of this embodiment can be applied to syngas synthesis C in Fe-based catalyst 2 、C 3 and other small molecule alkenes. The amount of active metal Fe loaded on the inner surface of the micro-reaction channel 7 is 17.5g / m 2 . Feed gas H 2 The / CO volume ratio is 2, the reaction temperature is 325°C, the pressure is 0.55MPa, and the volume space velocity is 3100h -1 .
[0075] Table 2 shows the comparison between the reactor used in this example and the axial reactor in the prior art. The catalytic reaction unit of two kinds of reac...
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