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A kind of preparation method of graphene composite material

A composite material and graphene technology, applied in the direction of heat exchange materials, chemical instruments and methods, carbon compounds, etc., can solve the problems of narrow commercial application fields and weak technology transformation ability, and achieve the effect of improving heat dissipation performance

Active Publication Date: 2019-06-18
山西晋尤特环境科技有限公司
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  • Summary
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At the same time, my country's graphene industry is still facing problems such as weak technology transformation capabilities and narrow commercial application fields.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] In step 1, 20 mg of graphite oxide was ground, mixed with 20 mL of diethylene glycol, and ultrasonically stripped for 1 h to obtain a GO dispersion.

[0019] Step 2, 23.32mg diethylene glycol solution containing 1.83mg zinc acetate is placed in the container, the GO diethylene glycol dispersion is added dropwise in the diethylene glycol solution of zinc acetate, magnetic After stirring evenly, add 0.029mg of hydrochloric acid and 0.54mg of distilled water drop by drop, continue to stir and react to obtain a sol, leave it to stand to form a gel, age for several days, wash and dry, roast at 350 °C for 2 hours, and grind to obtain a graphene material .

[0020] Step 3: Use a high-temperature PVT growth furnace to put the graphene material into a graphite crucible, first pass a 1:20 mixture of H2 and argon, and simultaneously raise the temperature to 1650°C and keep the temperature constant for 30 minutes, in order to eliminate the grinding process. mechanical damage cause...

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PUM

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Abstract

The invention provides a method for preparing a graphene composite material. The method comprises the following steps: firstly, mixing graphite oxide with condensed diethylene glycol so as to obtain a graphite oxide diethylene glycol dispersion; putting a diethylene glycol solution with zinc acetate into a container, dropping the graphite oxide diethylene glycol dispersion into the diethylene glycol solution with zinc acetate, dropping hydrochloric acid and distilled water dropwise, continuously stirring to implement a reaction so as to obtain sol, leaving to stand to obtain gel, aging for days, washing, drying, and grinding so as to obtain a graphene material; heating the graphene material in the presence of hydrogen and argon so as to remove mechanical damage; further cooling, vacuuming, and removing oxides on the surface; finally introducing argon, heating to certain temperature, further cooling, and taking out, thereby obtaining the graphene composite material. A graphite heat radiation fin made of the graphene composite material prepared by using the method is capable of effectively transferring heat and improving heat radiation performance, can be also used as a flexible surface heat radiation body material, and can meet heat radiation requirements of high-power and high-integration systems of different fields.

Description

technical field [0001] The invention belongs to the field of new materials, relates to a graphene composite material, in particular to a preparation method of a graphene composite material. Background technique [0002] Graphene is the thinnest material known so far; and it is not only light and thin, but also very strong and soft; graphene has high mechanical strength, good thermal conductivity and fast carrier mobility; graphene In recent years, as a new type of material, composite materials have been valued and applied by more and more people. [0003] There are many methods for the preparation of graphene composite materials, and this field has become a hot spot that scholars from all over the world have paid attention to, especially graphene composite materials have become the "star" of today's new materials. [0004] Graphene is a hexagonal honeycomb lattice planar film with a thickness of only one carbon atom. For "super material". Graphene has a wide range of uses...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B32/192C01B32/194C01B32/196C09K5/14
CPCC01P2006/80C09K5/14
Inventor 王帅
Owner 山西晋尤特环境科技有限公司
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