A kind of preparation method of graphene composite material
A composite material and graphene technology, applied in the direction of heat exchange materials, chemical instruments and methods, carbon compounds, etc., can solve the problems of narrow commercial application fields and weak technology transformation ability, and achieve the effect of improving heat dissipation performance
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[0018] In step 1, 20 mg of graphite oxide was ground, mixed with 20 mL of diethylene glycol, and ultrasonically stripped for 1 h to obtain a GO dispersion.
[0019] Step 2, 23.32mg diethylene glycol solution containing 1.83mg zinc acetate is placed in the container, the GO diethylene glycol dispersion is added dropwise in the diethylene glycol solution of zinc acetate, magnetic After stirring evenly, add 0.029mg of hydrochloric acid and 0.54mg of distilled water drop by drop, continue to stir and react to obtain a sol, leave it to stand to form a gel, age for several days, wash and dry, roast at 350 °C for 2 hours, and grind to obtain a graphene material .
[0020] Step 3: Use a high-temperature PVT growth furnace to put the graphene material into a graphite crucible, first pass a 1:20 mixture of H2 and argon, and simultaneously raise the temperature to 1650°C and keep the temperature constant for 30 minutes, in order to eliminate the grinding process. mechanical damage cause...
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