High-temperature lubricants
A high-temperature, high-temperature oil technology, used in high-temperature greases for continuous use temperatures up to 250 ° C, in the field of oils and greases, can solve problems such as long functional duration
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Embodiment 1 to 2
[0067] Preparation of high temperature oil according to the invention
[0068] The long-chain ester or aliphatically substituted naphthalene is preset in a stirred boiler. At 100° C., polyisobutene and optionally another oil are added thereto under stirring. Subsequently, the mixture was stirred for 1 h in order to obtain a homogeneous mixture. The antiwear additives and antioxidants were added to the boiler at 60°C with stirring. After about 1 hour, the finished oil can be filled into the provided containers.
[0069] Composition of high temperature oil:
[0070] Table 1
[0071]
[0072] Table 2
[0073]
[0074] Base data for the oil examples can be derived from Table 3.
[0075] table 3
[0076]
[0077] In addition, the friction properties of the oil were measured in SRV and the evaporative losses in dynamic TGA according to DIN 51834-2. The results are shown in Tables 4 and 5 and in figure 1 and 2 shown in the graph.
[0078] Table 4
[0079]
[008...
Embodiment 3 to 8
[0084] Preparation of high temperature grease according to the invention
[0085] The base oil is preset in the stirred boiler. Polyisobutene and optionally another oil and thickener are added thereto with stirring at 100°C.
[0086] The thickener is produced by in situ reaction of the reactants employed in the base oil. Subsequently, the mixture was heated to 150°C to 210°C, stirred for several hours and cooled again. During cooling, at about 60°C, the required antiwear additives, antioxidants and anticorrosion additives are added thereto. A homogeneous mixture of greases is obtained by a final homogenization step via rollers, colloid mill or Gaulin.
[0087] The composition of the high temperature grease is shown in Table 6.
[0088] Table 6
[0089]
[0090]
Embodiment 3
[0092] Example 3: LiOH, 12-hydroxystearic acid, azelaic acid
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