Liquid grouting material used for coke oven furnace wall crack hot repairing, and preparation method and application method thereof

A technology of hot repairing and grouting materials, applied in the direction of preventing/repairing the leakage of bricklaying, can solve the problems of reduced working life of blast furnace, no bonding strength, strong smell of curing agent, etc., and achieve good impermeability and high temperature resistance. , Good mechanical strength and bond strength, good high temperature thermal stability

Active Publication Date: 2017-12-08
SHANGHAI INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If effective control measures are not taken in time, it will not only affect the normal operation of the blast furnace, reduce the working life of the blast furnace, and affect the output; but also have a bad impact on the surrounding environment, endangering the health and personal safety of the surrounding workers.
[0004] In Chinese patents CN101654354 B and CN101597497 B, diethylene glycol ethyl ether acetate and glyceryl triacetate are respectively used as curing agents. After curing with water glass, the serous calculus rate is low, and a certain proportion of water remains in the upper part of the calculus body; the serous The stone body is in the form of white powder, and the cementation strength of the pure stone body is almost non-existent; after the stone body is solidified, it is easy to lose water and shrink, and t

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] A liquid grouting material used for thermal repair of coke oven wall cracks, calculated by parts by mass, its raw material composition and content are as follows:

[0049] 100 parts of water glass;

[0050] 100 parts of solid filler;

[0051] 9 parts of additives;

[0052] The water glass is sodium water glass with a modulus range of 3.1 to 3.4 and a Baume degree of Bé=38;

[0053] The solid filler is a mixture of mullite, refractory clay and quartz sand, the amount of mullite, refractory clay and quartz sand in the mixture is calculated by mass percentage, mullite: refractory clay: quartz sand is 70 %: 20%: 10%;

[0054] Wherein, the mullite molecular formula is 3Al 2 o 3 ·2S i o 2 , the refractoriness is 1800℃, and the average bulk density is 1.911g / mL;

[0055] Described refractory clay is soft clay, and its molecular formula is Al 2 o 3 2SiO2 2 2H 2 O, where Al 2 o 3 Content1580℃, average bulk density is 1.199g / mL;

[0056] The quartz sand is ordinary...

Embodiment 2

[0072] A liquid grouting material used for thermal repair of coke oven wall cracks, calculated by parts by mass, its raw material composition and content are as follows:

[0073] 100 parts of water glass;

[0074] 250 parts of solid filler;

[0075] 16 parts of additives;

[0076] The water glass is sodium water glass with a modulus range of 3.1 to 3.4 and a Baume degree of Bé=38;

[0077] The solid filler is a mixture of mullite, refractory clay and quartz sand, the amount of mullite, refractory clay and quartz sand in the mixture is calculated by mass percentage, mullite: refractory clay: quartz sand is 50 %: 30%: 20%;

[0078] Wherein, the mullite molecular formula is 3Al 2 o 3 ·2S i o 2 , the refractoriness is 1800℃, and the average bulk density is 1.911g / mL;

[0079] Described refractory clay is soft clay, and its molecular formula is Al 2 o 3 2SiO2 2 2H 2 O, where Al 2 o 3 Content1580℃, average bulk density is 1.199g / mL;

[0080] The quartz sand is ordinar...

Embodiment 3

[0096] A liquid grouting material for thermal repair of coke oven wall cracks, calculated by parts by mass, its raw material composition and content are as follows:

[0097] 100 parts of water glass;

[0098] 180 parts of solid filler;

[0099] 13 parts of additives;

[0100] The water glass is sodium water glass with a modulus range of 3.1 to 3.4 and a Baume degree of Bé=38;

[0101] The solid filler is a mixture of mullite, refractory clay and quartz sand, the amount of mullite, refractory clay and quartz sand in the mixture is calculated by mass percentage, mullite: refractory clay: quartz sand is 60 %: 25%: 15%;

[0102] Wherein, the mullite molecular formula is 3Al 2 o 3 ·2S i o 2 , the refractoriness is 1800℃, and the average bulk density is 1.911g / mL;

[0103] Described refractory clay is soft clay, and its molecular formula is Al 2 o 3 2SiO2 2 2H 2 O, where Al 2 o 3 Content1580℃, average bulk density is 1.199g / mL;

[0104] The quartz sand is ordinary qua...

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Abstract

The invention discloses a liquid grouting material used for coke oven furnace wall crack hot repairing, and a preparation method thereof. The liquid grouting material used for coke oven furnace wall crack hot repairing is composed of, by mass, 100 parts of water glass, 100 to 250 parts of a solid filling material, and 9 to 16 parts of an additive. The solid filling material is composed of, by mass, 50 to 70% of mullite, 20 to 30% of refractory clay, and 10 to 20% of quartz sand. The additive is composed of a dispersant, a penetrant, and an antifoaming agent. According to the preparation method, the additive and the solid filling material are added into a water glass solution successively for uniform mixing so as to obtain the liquid grouting material used for coke oven furnace wall crack hot repairing. The liquid grouting material used for coke oven furnace wall crack hot repairing is convenient for pumping, possesses excellent cohesiveness with refractory material to be repaired, is wide in curing sintering temperature range, and is convenient for construction; the raw materials are cheap and easily available; no harm on human body is caused; the preparation period is short; the preparation method is simple; production cost is low; the production process is friendly to the environment; no pollution is caused; and large scale production can be realized.

Description

technical field [0001] The invention relates to a liquid grouting material for hot repair of coke oven wall cracks, a preparation method and a use method, especially a heat-resistant high-strength non-shrinkage grouting material used in a high-temperature environment, which can be widely used in high-temperature facilities such as coke ovens The filling and repairing of wall cracks belongs to the coking field in the metallurgical coal chemical industry. Background technique [0002] In the long-term use of coke oven, it is affected by high temperature, mechanical and physical and chemical reactions, and the furnace body always tends to be gradually aging and damaged. After the start of production, due to the temperature shock of sudden changes in cold and heat caused by operations such as opening and closing of the furnace door, coal loading and coking, mechanical collision, extrusion, friction, and the erosion of certain harmful substances in the gas, various parts of the f...

Claims

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Application Information

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IPC IPC(8): C04B35/66C10B29/06
CPCC04B35/66C04B2235/3418C04B2235/3427C04B2235/3463C04B2235/349C04B2235/96C10B29/06
Inventor 陆王钊金双玲金鸣林唐珊胡震张建勇
Owner SHANGHAI INST OF TECH
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