Pavement material with wide phase change temperature zone and preparation method thereof
A technology of pavement materials and shape-setting phase change materials, which is applied in the field of pavement materials and its preparation in a wide phase change temperature range, can solve the problems of large influence of seasons and weather changes, poor durability, and temperature changes, so as to delay the peak occurrence time, Effect of improving durability and prolonging life
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Embodiment 1
[0014] The phase change material carrier mesoporous silica SBA-15 is commercially available.
[0015] Example 1
[0016] Separately add 0.1g of tetradecane, pentadecane, hexadecane, heptadecane, octadecane, nonadecane, eicosane, polyethylene glycol (molecular weight 2000) into 100ml of absolute ethanol and heat and stir to prepare 1g / L tetradecane, pentadecane, hexadecane, heptadecane, octadecane, nonadecane, eicosane, polyethylene glycol (molecular weight 2000) ethanol solution, and then add 45mg SBA-15 separately In the above-mentioned phase change material core material solution, the mixture was stirred at 65°C for 4h, and then dried at 80°C for 24h, to obtain the shaped phase change material tetradecane / SBA-15, pentadecane / SBA-15, ten Hexane / SBA-15, heptadecane / SBA-15, octadecane / SBA-15, nonadecane / SBA-15, eicosane / SBA-15, polyethylene glycol / SBA-15.
[0017] Take 1g each of the above-mentioned wide phase change temperature zone composite shaped phase change materials at differ...
Embodiment 2
[0019] Add 0.08g of phase change material core material tetradecane, pentadecane, hexadecane, heptadecane, octadecane, nonadecane, eicosane, polyethylene glycol (molecular weight 2000) into 100ml absolute ethanol Medium heating and stirring, prepare 1g / L tetradecane, pentadecane, hexadecane, heptadecane, octadecane, nonadecane, eicosane, polyethylene glycol (molecular weight 2000) ethanol solution, and then mix 45mg SBA-15 was added to the above-mentioned phase change material core material solution, and the mixture was stirred at 65°C for 4 hours, and then dried at 80°C for 24 hours to obtain the shaped phase change material tetradecane / SBA-15 and pentadecane / SBA-15, hexadecane / SBA-15, heptadecane / SBA-15, octadecane / SBA-15, nonadecane / SBA-15, eicosane / SBA-15, polyethylene glycol / SBA -15.
[0020] Combine the above-mentioned wide phase change temperature zone with different temperatures and composite shape-stable phase change materials tetradecane / SBA-15 1g, pentadecane / SBA-151...
Embodiment 3
[0022] Add 0.06g phase change material core material tetradecane, pentadecane, hexadecane, heptadecane, octadecane, nonadecane, eicosane, polyethylene glycol (molecular weight 2000) into 100ml absolute ethanol Medium heating and stirring, prepare 1g / L tetradecane, pentadecane, hexadecane, heptadecane, octadecane, nonadecane, eicosane, polyethylene glycol (molecular weight 2000) ethanol solution, and then mix 45mg SBA-15 was added to the above-mentioned phase change material core material solution, and the mixture was stirred at 65°C for 4 hours, and then dried at 80°C for 24 hours to obtain the shaped phase change material tetradecane / SBA-15 and pentadecane / SBA-15, hexadecane / SBA-15, heptadecane / SBA-15, octadecane / SBA-15, nonadecane / SBA-15, eicosane / SBA-15, polyethylene glycol / SBA -15.
[0023] Take 1g of each of the above-mentioned shaped phase change materials and mix them thoroughly to prepare a composite shaped phase-change material with a wide phase change temperature rang...
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