Method for controlling water activity and application thereof
A moisture and activity technology, used in material inspection products, testing food, etc., can solve problems such as difficulty in meeting experimental needs and large humidity effects
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Embodiment 1
[0072] Example 1 According to the experimental requirements, prepare the required saturated salt solution
[0073] Under the condition of 25°C, the water activity values that can be precisely controlled by this method are 0.064, 0.113, 0.328, 0.4320.529, 0.576, 0.649, 0.709, 0.743, 0.753, 0.809, 0.810, 0.843, 0.851, 0.902, 0.936 and 0.973. According to the needs of the experiment, refer to Table 1 to prepare the required saturated salt solution.
[0074] Table 1 Water activity value produced by saturated salt solution at 25°C
[0075] Numbering
Types of supersaturated salt solutions
Aw(25℃)
1
Lithium bromide saturated solution
0.064
2
Lithium chloride saturated solution
0.113
3
Magnesium chloride saturated solution
0.328
4
Potassium Carbonate Saturated Solution
0.432
5
Saturated solution of magnesium nitrate
0.529
6
Sodium bromide saturated solution
0.576
7
Saturated Cob...
Embodiment 2
[0094] The adjustment of embodiment 2 sample water activity
[0095] The water activity of the sample needs to be adjusted to the target water activity. The specific operations used are as follows:
[0096] A universal pulverizer is used to grind and pulverize the sample, and then n different amounts of water are added to the ground sample, wherein the number of n is 6-10. Under the condition of 4°C, equilibrate overnight, adopt Aqualab 4TE (Decagon Devices, the United States, the accuracy is ± 0.005) to measure the water activity of the sample after equilibration, and use Moisture Analyzer MJ33 (MettlerToledo, Switzerland) to measure the moisture content of the sample after equilibration, Take the water content as the ordinate and the water activity as the abscissa to establish the water activity-moisture content curve. According to the curve, calculate the amount of sterile water that needs to be added for the target water activity of the sample experiment, and use it for ...
Embodiment 3
[0097] Embodiment 3 water activity control accuracy monitoring
[0098]Randomly select two target water activities of 0.843 and 0.936 for accuracy monitoring.
[0099] When the target water activity is 0.843, add saturated potassium chloride solution at the bottom of the drier. The amount of saturated potassium chloride solution added should be no less than 10% of the volume of the drier and no more than the separator of the drier. Adjust 100g of corn with water activity to 0.843, and divide it into four parts and place it on a dry partition (such as figure 1 shown). Move in parallel along the upper opening of the desiccator, cover the desiccator cover coated with petroleum jelly, and place it in a constant temperature incubator at 25°C. Set up three replicates.
[0100] When the target water activity is 0.936, add saturated potassium nitrate solution at the bottom of the drier. The amount of saturated potassium nitrate solution added should not be less than 10% of the volu...
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