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A kind of preparation method of shear force thermal deformation mold and NdFeB magnet

A technology of neodymium iron boron and thermal deformation, which is applied in the direction of inductance/transformer/magnet manufacturing, magnetic objects, magnetic materials, etc., can solve the problems of reducing magnetic performance, grain growth, and magnet difficulties with large deformation and deformation, and achieves Promote grain boundary slip, improve magnetic properties, anisotropy, and magnetic property promotion effects

Active Publication Date: 2020-10-16
BEIJING UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, there are many patents for all thermally deformed NdFeB magnets, such as patents CN102744406A, CN104103414A, CN105869876A, etc. These methods are all completed under positive pressure. If you want to obtain a large deformation magnet, you often need to increase the temperature and increase the temperature grain. Will grow and reduce magnetic properties
It is difficult to obtain a magnet with large deformation deformation without increasing the temperature

Method used

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  • A kind of preparation method of shear force thermal deformation mold and NdFeB magnet
  • A kind of preparation method of shear force thermal deformation mold and NdFeB magnet
  • A kind of preparation method of shear force thermal deformation mold and NdFeB magnet

Examples

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Effect test

Embodiment 1

[0032] A kind of 0 ° inclination angle thermally deformable magnet preparation, implements according to the following steps:

[0033] The first step is to put the prepared commercial F powder into The hard alloy mold is placed in a spark plasma sintering furnace for sintering to obtain an isotropic hot-pressed magnet. The specific sintering process is as follows: the heating rate is 50-80° C. / min, the sintering temperature is 650° C. and the temperature is kept for 3 minutes, and the pressure is 300 MPa.

[0034] In the second step, take out the magnet obtained in the first step, and use wire cutting to directly cut out a 0° angle to obtain the required cylinder.

[0035] The third step is to remove impurities on the surface of the oblique cylinder, put it into a graphite mold at 0°, use spark plasma sintering, and deform the hot-pressed magnet with appropriate temperature and pressure to obtain an anisotropic hot-deformed magnet. The specific sintering process is as follow...

Embodiment 2

[0037] A kind of 5 ° inclination angle thermally deformable magnet preparation, implements according to the following steps:

[0038] The first step is to put the prepared commercial F powder into The hard alloy mold is placed in a spark plasma sintering furnace for sintering to obtain an isotropic hot-pressed magnet. The specific sintering process is as follows: the heating rate is 50-80° C. / min, the sintering temperature is 650° C. and the temperature is kept for 3 minutes, and the pressure is 300 MPa.

[0039] In the second step, take out the magnet obtained in the first step, and use wire cutting to directly cut out a 5° angle to obtain the required cylinder.

[0040]The third step is to remove impurities on the surface of the oblique cylinder, put it into a 5° graphite mold, use spark plasma sintering, and use suitable temperature and pressure to deform the hot-pressed magnet to obtain an anisotropic hot-deformed magnet. The specific sintering process is as follows: th...

Embodiment 3

[0042] A kind of 10 ° inclination angle thermally deformable magnet preparation, implements according to the following steps:

[0043] The first step is to put the prepared commercial F powder into The hard alloy mold is placed in a spark plasma sintering furnace for sintering to obtain an isotropic hot-pressed magnet. The specific sintering process is as follows: the heating rate is 50-80° C. / min, the sintering temperature is 650° C. and the temperature is kept for 3 minutes, and the pressure is 300 MPa.

[0044] In the second step, take out the magnet obtained in the first step, and use wire cutting to directly cut out a 10° angle to obtain the required cylinder.

[0045] The third step is to remove impurities on the surface of the oblique cylinder, put it into a 10° graphite mold, use spark plasma sintering, and use suitable temperature and pressure to deform the hot-pressed magnet to obtain an anisotropic hot-deformed magnet. The specific sintering process is as follows...

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Abstract

A thermal deformation mold with shear force and a preparation method for a neodymium-iron-boron magnet, relating to the field of rare-earth permanent magnets. The obtaining of the shear force depends on a particular angle between a sample and a mold contact surface, and the magnitude of the shear force is controlled by adjusting the magnitude of the angle. A compact thermal deformation magnet with high deformation is prepared by loading rapidly-quenched powder into the mold, using a spark plasma sintering system (SPS), and controlling the sintering conditions. The deformation of the neodymium-iron-boron magnet is greatly promoted by means of the addition of the shear force, the deformation efficiency is improved, and the magnetic property is improved.

Description

technical field [0001] This patent invents a method for preparing a thermally deformed mold with added shear force and an NdFeB magnet, which belongs to the field of rare earth permanent magnets. Background technique [0002] In 1984, researchers in Japan and the United States prepared NdFeB (2:14:1) permanent magnets with a tetragonal structure by using powder metallurgy and rapid quenching respectively, thus announcing the birth of the third generation of rare earth permanent magnet materials. Today, NdFeB permanent magnets are still the permanent magnets with the best performance, known as the "magnet king". [0003] As the third generation of rare earth permanent magnets, NdFeB magnets have the advantages of high performance, high magnetic energy product and cost performance, and are widely used in many fields such as machinery, information, energy, transportation, etc., and have become the core of modern industry and science and technology. One of the supporting materi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01F41/02H01F1/057B22F3/14B22F3/105
CPCB22F3/105B22F3/14H01F1/057H01F41/02
Inventor 路清梅钮建岳明李玉卿徐云鹏刘卫强张东涛
Owner BEIJING UNIV OF TECH