Comprehensive extraction method of biological salt and betacyanin from suaeda salsa
A technology of betalain and Suaeda salsa, applied in chemical instruments and methods, food science, azo dyes, etc., can solve the problems of low yield, low product purity, and no reports on simultaneous extraction processes or methods. , to achieve the effect of improving purity, short processing time and preventing degradation
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example 1
[0027] A method for comprehensively extracting Suaeda salsa biological salt and betaine, comprising the following steps:
[0028] (1) raw material pretreatment: the freshly picked Suaeda salina stems and leaves are washed and dried, and an extraction solvent (40% ethanol and 0.1M citric acid with a volume concentration of 1:5) is added according to the ratio of solid to liquid Mixed according to the ratio of 1:0.5), flash extraction (extraction time is 1.5min, extraction temperature is 25°C, extraction voltage is 180v), filtered, and supernatant and precipitate are collected respectively;
[0029] (2) Ultrasound-assisted enzymolysis treatment: get the precipitate that step (1) collects, add the compound enzyme (by pectinase, cellulase, neutral protease and α-glucosidase according to 1:2:1:1 ratio), mix well, adjust pH, after ultrasonic treatment (ultrasonic power 220W, ultrasonic time 5min) for enzymolysis reaction (enzymolysis condition is pH3.5, temperature 25 °C, the enzym...
example 2
[0035] A method for comprehensively extracting Suaeda salsa biological salt and betaine, comprising the following steps:
[0036] (1) raw material pretreatment: the freshly picked Suaeda salsa stems and leaves are washed and dried, and an extraction solvent (45% ethanol and 0.3M citric acid with a volume concentration of 1:8) is added according to the ratio of solid to liquid Mixed according to the ratio of 1:0.5), flash extraction (extraction time is 2min, extraction temperature is 28°C, extraction voltage is 185v), filtered, and supernatant and precipitate are collected respectively;
[0037] (2) Ultrasound-assisted enzymolysis treatment: get the precipitate that step (1) collects, add the compound enzyme (by pectinase, cellulase, neutral protease and α-glucosidase according to 2:3:2:1.5 ratio), mix well, adjust pH, after ultrasonic treatment (ultrasonic power 260W, ultrasonic time 8min) for enzymolysis reaction (enzymolysis condition is pH3.5, temperature 28 °C, the enzyma...
example 3
[0043] A method for comprehensively extracting Suaeda salsa biological salt and betaine, comprising the following steps:
[0044] (1) raw material pretreatment: the freshly picked Suaeda salsa stems and leaves are washed and dried, and an extraction solvent (75% ethanol and 0.45M citric acid with a volume concentration of 1:10) is added according to the ratio of solid to liquid Mixed according to the ratio of 1:0.5), flash extraction (extraction time is 4min, extraction temperature is 28.5°C, extraction voltage is 202v), filtered, and supernatant and precipitate are collected respectively;
[0045] (2) Ultrasound-assisted enzymolysis treatment: get the precipitate that step (1) collects, add the compound enzyme (by pectinase, cellulase, neutral protease and α-glucosidase according to 4.5:6:5:2.7 ratio), mix well, adjust pH, after ultrasonic treatment (ultrasonic power is 420W, ultrasonic time is 12min) for enzymolysis reaction (enzymolysis condition is pH6.2, temperature 36 ℃...
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