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Laser photoacoustic compound detection method for elements and defects and system thereof

A composite detection and laser technology, applied in the direction of optical testing flaws/defects, measuring devices, thermal excitation analysis, etc., can solve problems such as long analysis time, high detection cost, and inability to detect element distribution, so as to reduce costs and improve detection efficiency , Improve the effect of detection accuracy

Inactive Publication Date: 2018-01-19
HUAZHONG UNIV OF SCI & TECH
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  • Abstract
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Problems solved by technology

[0008] In summary, although LIBS technology has superior performance in element detection, LIBS technology has not been applied to detect structural defects of materials at present.
Although laser ultrasonic testing technology has superior performance in non-destructive testing, it cannot detect element distribution
It can be seen that at present, the elements and defects of materials are analyzed separately by a single technical means, which takes a long time for analysis and high detection cost.
[0009] So far, there is no report on simultaneous detection of material elements and defects

Method used

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  • Laser photoacoustic compound detection method for elements and defects and system thereof

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Embodiment 1

[0043] Now take the detection of steel welds as an example to illustrate the use process of the laser photoacoustic composite detection system of the present invention. The specific operation steps are as follows:

[0044] (1) The pulsed laser 3 is a Nd:YAG Q-switched laser with an emission wavelength of 532 nm, a pulse duration of 6 ns, and an adjusted pulse energy of about 40 mJ. The water immersion ultrasonic probe 13 is focused on a non-focal plane with a frequency of 20 MHz. The model of the digital delay generator 11 is DG535, and its delay resolution is 5Ps.

[0045] (2) Place the welding sample on the 3D displacement platform 5 . The scanning surface is facing the laser light outlet, adjust the position of the 3D translation platform 5 in the X-axis direction and the position of the focusing objective lens 10, so that the pulsed laser beam is focused at the defocus amount -1mm position; adjust the position of the 3D translation platform 5 on the Y-Z axis To the initi...

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Abstract

Belonging to the laser material detection field, the invention discloses a laser photoacoustic compound detection method for elements and defects and a system thereof. A pulsed laser is incident to ananalysis sample to generate plasma and ultrasonic wave for simultaneous analysis of sample elementary composition and structural defects. The detection system comprises the pulsed laser, a spectrum detection unit, an ultrasonic detection unit, a sample stage unit and an analysis control unit. The analysis control unit comprises a digital time delayer and a computer, the digital time delayer is connected to the computer, the sample stage unit includes a 3D displacement platform, the 3D displacement platform s electrically connected to the digital time delayer, pulse laser emitted by the pulsedlaser is incident to a to-be-analyzed sample to produce plasma and ultrasonic wave simultaneously, the ultrasonic detection unit is used for detection of ultrasonic wave, and the spectrum detection unit is used for detection of a visible light spectrum emitted by plasma flame. The method and device provided by the invention can realize detection and analysis of sample elements and defects simultaneously.

Description

technical field [0001] The invention belongs to the field of laser material detection, and specifically relates to a compound detection method and system for element composition and defect distribution excited by laser, which mainly detects and analyzes light and sound signals generated after material excitation by laser to realize target detection. The elements and defects of the material are detected at the same time. Background technique [0002] In the field of material testing, element content and structural defects are two important aspects of material physical and chemical property testing. [0003] In terms of elemental analysis, traditional detection methods include chemical analysis, XRF, ICP-OES, etc. However, these methods have the disadvantages of destroying the sample and taking a long time, and cannot meet the needs of modern element detection such as fast, in-situ, minimally destructive or even non-destructive, so a new spectral detection technology-Laser In...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/71G01N21/17G01N21/88
Inventor 郭连波罗为马浴阳熊伟余云新马世祥褚燕武李祥友曾晓雁
Owner HUAZHONG UNIV OF SCI & TECH
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