A kind of anti-precipitation modified silicon dioxide and its preparation method and application
A silica and anti-precipitation technology, applied in the coating and other directions, can solve the problems such as the inability to fully disperse silica, the inability to meet the application performance, and the reduction of the proportion of silica, to achieve superior anti-precipitation performance and uniform modification treatment. , The effect of pigment absorption and balance
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Embodiment 1
[0043] A modified silicon dioxide modified by an acrylic acid copolymer can be prepared by the following method:
[0044]Add 100 kg of silica substrate into the double power mixer, the silica substrate selected is silica dry powder (i.e. white carbon black dry powder) prepared by precipitation method, keep mixed state, stir for 10min, then acrylic acid copolymer 1kg of DISPER2008 and 0.5kg of organic solvent are stirred evenly, atomized by a pressure pump, sprayed evenly into the mixer, kept stirring for 2.5h, and the mixed material is subjected to ultra-fine airflow pulverization, and the average particle size is controlled to 3.5μm to obtain modified Silica finished product 1, can be used as an oil paint additive.
[0045] Wherein, the organic solvent refers to a mixture of the following components in mass percentage: 75% xylene, 15% cyclohexanone and 10% ethylene glycol. Most of the organic solvent is volatilized during the superjet milling process, and the addition of the...
Embodiment 2
[0047] A modified silicon dioxide modified by a polycarboxylic acid copolymer can be prepared by the following method:
[0048] Add 120kg of silica base material to the double power mixer, the silica base material selected is silica dry powder prepared by macroporous silica gel method, keep the mixed state, stir for 10min, mix polycarboxylic acid copolymer DISPER104 18kg with organic 10 kg of solvent was stirred evenly and atomized by a pressure pump, then evenly sprayed into the mixer, kept stirring for 3 hours, and the mixed material was subjected to ultra-fine airflow pulverization, and the average particle size was controlled to 5.5 μm to obtain the finished product 2 of modified silica. Can be used as an oil paint additive.
[0049] Wherein, the organic solvent refers to a mixture of the following components in mass percentage: 75% xylene, 10% cyclohexanone and 15% ethylene glycol. Most of the organic solvent is volatilized during the superjet milling process, and the ad...
Embodiment 3
[0051] A modified silicon dioxide modified by an acrylic copolymer, which can be prepared by the following method:
[0052] Mix and stir 300kg of silica substrate and 700kg of water to form a slurry, stir for 2 hours, add acetic acid to adjust the pH value to 4.5, stir evenly, and keep stirring. Add 30 kg of acrylic copolymer DISPER2009, keep stirring for 2 hours, dry to control the moisture content to ≤4.5%, make the slurry into a base material, and process it into a finished product with ultra-fine airflow pulverization, with an average particle size of 6.5 μm, to obtain the finished product 3 of modified silica, Can be used as water-based paint additive.
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