Ink, ink container, Liquid Discharging Device, and Image Forming Method and apparatus thereof
An ink and organic solvent technology, which is applied in the field of liquid discharge devices, can solve the problems of beading (beading, insufficient ink absorption, transfer of the image part to the side of the joint paper, etc.), and achieves the effect of good image fixability and discharge stability.
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preparation example 1
[0532] -Preparation of Surface Modified Black Pigment Dispersion (1)-
[0533] BlackPearls (registered trademark) 1000 (having a BET specific surface area of 150m) manufactured by Cabot Corporation 2 / g and DBPA 105mL / 100g carbon black) 100g, sulfanilic acid 100mmol, and ion-exchange high-purity water 1L were mixed with a Silverson mixer (6000rpm) at room temperature.
[0534] When the pH value of the obtained slurry was higher than 4, 100 mmol of nitric acid was added to the slurry. Thirty minutes later, sodium nitrite (100 mmol) dissolved in a small amount of ion-exchanged high-purity water was gradually added to the above mixture. Furthermore, the product was heated to 60 degreeC with stirring, and it was made to react for 1 hour.
[0535] Subsequently, the pH of the resultant was adjusted to 9 with a 10% by mass tetrabutylammonium hydroxide solution (methanol solution), thereby obtaining a modified pigment dispersion containing at least one sulfanilic acid after 30 min...
preparation example 2
[0539] -Preparation of Surface Modified Black Pigment Dispersion (2)-
[0540] In the ProcessALL 4HV mixer (4L), BlackPearls (registered trademark) 880 (having a BET specific surface area of 220m 2 / g and DBPA 105mL / 100g of carbon black) 500g, to which 1L of ion-exchange high-purity water and 1mol of 4-aminobenzoic acid were added. Next, the resulting mixture was vigorously mixed at 300 rpm for 10 minutes and heated to 60 °C. A 20% by mass sodium nitrite aqueous solution [1 mol equivalent of 4-aminobenzoic acid] was added thereto over 15 minutes. The resulting mixture was mixed and stirred for 3 hours, and heated to 60°C. The above reactant was taken out while being diluted with 750 mL of ion-exchanged high-purity water.
[0541] Subsequently, the pH of the resultant was adjusted to 9 with a 10% by mass tetrabutylammonium hydroxide solution (methanol solution) to obtain a modified pigment dispersion containing at least one aminobenzene Formate- or tetraethylammonium-amin...
preparation example 3
[0545] -Preparation of Surface Modified Black Pigment Dispersion (3)-
[0546] In the ProcessALL 4HV mixer (4L), BlackPearls (registered trademark) 880 (having a BET specific surface area of 220m 2 / g and DBPA 105mL / 100g of carbon black) 500g, to which 1L of ion-exchanged high-purity water and 175mmol of 4-aminobenzoic acid were added. Next, the resulting mixture was vigorously mixed at 300 rpm for 10 minutes and heated to 60 °C. A 20% by mass sodium nitrite aqueous solution [175 mmol equivalent of 4-aminobenzoic acid] was added thereto over 15 minutes. The resulting mixture was mixed and stirred for 3 hours, and heated to 60°C. The above reactant was taken out while being diluted with 750 mL of ion-exchanged high-purity water.
[0547] Subsequently, the pH of the resultant was adjusted to 9 with a 10% by mass tetraethylammonium hydroxide solution to obtain a modified pigment dispersion comprising at least one aminobenzoic acid group after 30 minutes. or tetraethylammoni...
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