High-temperature superconducting film material and manufacturing method thereof
A technology of high temperature superconducting thin film and manufacturing method, which can be applied to the usage of superconducting elements, superconducting devices, superconducting/high conducting conductors, etc., can solve problems such as unworkability from an economic point of view, widen the scope of application and reduce production costs , the effect of improving the current carrying capacity
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Embodiment 1
[0024] A high-temperature superconducting thin film material is composed of the following components according to mass percentage: 2.9% yttrium trifluoroacetate, 3.0% copper trifluoroacetate, 5.8% barium trifluoroacetate, 2.5% terpineol, 10.5% Acetylacetone, 6.5% zirconium acetylacetonate and the balance niobium. During preparation, mix yttrium hydrochloric acid solution, barium hydrochloric acid solution, titanium hydrochloric acid solution, zirconium hydrochloric acid solution and niobium hydrochloric acid solution evenly, stir with a magnetic stirrer for 1-3 hours, remove water, and obtain pure gel; add terpineol, Precursor solution is prepared, and coated on the substrate for low-temperature thermal decomposition; after the treated substrate is heat-treated, annealing heat treatment is performed, and the annealing heat treatment time is 1.5 hours, and a high-temperature superconducting thin film material is obtained.
Embodiment 2
[0026] A high-temperature superconducting thin film material is composed of the following components according to mass percentage: 3.3% yttrium trifluoroacetate, 3.4% copper trifluoroacetate, 6.8% barium trifluoroacetate, 2.5% terpineol, 11.5% Acetylacetone, 6.5% zirconium acetylacetonate and the balance niobium. During preparation, mix yttrium hydrochloric acid solution, barium hydrochloric acid solution, titanium hydrochloric acid solution, zirconium hydrochloric acid solution and niobium hydrochloric acid solution evenly, stir with a magnetic stirrer for 1-3 hours, remove water, and obtain pure gel; add terpineol, Precursor solution is prepared, and coated on the substrate for low-temperature thermal decomposition; after the treated substrate is heat-treated, annealing heat treatment is performed, and the annealing heat treatment time is 1.5 hours, and a high-temperature superconducting thin film material is obtained.
Embodiment 3
[0028] A high-temperature superconducting thin film material is composed of the following components according to mass percentage: 3.9% yttrium trifluoroacetate, 4.0% copper trifluoroacetate, 5.8% barium trifluoroacetate, 2.5% terpineol, 12.5% Acetylacetone, 7.5% zirconium acetylacetonate and the balance niobium. During preparation, mix yttrium hydrochloric acid solution, barium hydrochloric acid solution, titanium hydrochloric acid solution, zirconium hydrochloric acid solution and niobium hydrochloric acid solution evenly, stir with a magnetic stirrer for 1-3 hours, remove water, and obtain pure gel; add terpineol, Precursor solution is prepared, and coated on the substrate for low-temperature thermal decomposition; after the treated substrate is heat-treated, annealing heat treatment is performed, and the annealing heat treatment time is 1.5 hours, and a high-temperature superconducting thin film material is obtained.
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