High-temperature superconducting film material and manufacturing method thereof

A technology of high temperature superconducting thin film and manufacturing method, which can be applied to the usage of superconducting elements, superconducting devices, superconducting/high conducting conductors, etc., can solve problems such as unworkability from an economic point of view, widen the scope of application and reduce production costs , the effect of improving the current carrying capacity

Inactive Publication Date: 2018-02-23
蒋艳玲
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But this method has encountered many difficulties when it comes to practical application, the irradiated material is radioactive, and it is not feasible from an economic point of view

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A high-temperature superconducting thin film material is composed of the following components according to mass percentage: 2.9% yttrium trifluoroacetate, 3.0% copper trifluoroacetate, 5.8% barium trifluoroacetate, 2.5% terpineol, 10.5% Acetylacetone, 6.5% zirconium acetylacetonate and the balance niobium. During preparation, mix yttrium hydrochloric acid solution, barium hydrochloric acid solution, titanium hydrochloric acid solution, zirconium hydrochloric acid solution and niobium hydrochloric acid solution evenly, stir with a magnetic stirrer for 1-3 hours, remove water, and obtain pure gel; add terpineol, Precursor solution is prepared, and coated on the substrate for low-temperature thermal decomposition; after the treated substrate is heat-treated, annealing heat treatment is performed, and the annealing heat treatment time is 1.5 hours, and a high-temperature superconducting thin film material is obtained.

Embodiment 2

[0026] A high-temperature superconducting thin film material is composed of the following components according to mass percentage: 3.3% yttrium trifluoroacetate, 3.4% copper trifluoroacetate, 6.8% barium trifluoroacetate, 2.5% terpineol, 11.5% Acetylacetone, 6.5% zirconium acetylacetonate and the balance niobium. During preparation, mix yttrium hydrochloric acid solution, barium hydrochloric acid solution, titanium hydrochloric acid solution, zirconium hydrochloric acid solution and niobium hydrochloric acid solution evenly, stir with a magnetic stirrer for 1-3 hours, remove water, and obtain pure gel; add terpineol, Precursor solution is prepared, and coated on the substrate for low-temperature thermal decomposition; after the treated substrate is heat-treated, annealing heat treatment is performed, and the annealing heat treatment time is 1.5 hours, and a high-temperature superconducting thin film material is obtained.

Embodiment 3

[0028] A high-temperature superconducting thin film material is composed of the following components according to mass percentage: 3.9% yttrium trifluoroacetate, 4.0% copper trifluoroacetate, 5.8% barium trifluoroacetate, 2.5% terpineol, 12.5% Acetylacetone, 7.5% zirconium acetylacetonate and the balance niobium. During preparation, mix yttrium hydrochloric acid solution, barium hydrochloric acid solution, titanium hydrochloric acid solution, zirconium hydrochloric acid solution and niobium hydrochloric acid solution evenly, stir with a magnetic stirrer for 1-3 hours, remove water, and obtain pure gel; add terpineol, Precursor solution is prepared, and coated on the substrate for low-temperature thermal decomposition; after the treated substrate is heat-treated, annealing heat treatment is performed, and the annealing heat treatment time is 1.5 hours, and a high-temperature superconducting thin film material is obtained.

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PUM

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Abstract

The invention relates to a high-temperature superconducting film material and a manufacturing method thereof. The high-temperature superconducting film material is prepared from the following ingredients in percentage by mass: 2.2 to 4.0 percent of yttrium trifluoroacetate, 3.0 to 4.0 percent of copper trifluoroacetate, 4.8 to 7.8 percent of barium trifluoroacetate, 2.3 to 3.5 percent of terpilenol, 9.0 to 13.0 percent of titanium acetylacetone, 5.5 to 8.0 percent of zirconium acetylacetone and the balance of niobium. During the preparation, the method comprises the following steps of providing various hydrochloric acid solutions; performing uniform mixing; performing stirring; removing moisture to obtain pure gel; adding terpilenol to prepare precursor liquid; spraying the precursor liquid on a substrate, and performing low-temperature thermal decomposition; after thermal treatment, performing annealing heat treatment. The inventor performs a large number of ingredient and consumptionscreening experiments at the earlier stage, and accidentally finds that the current carrying capacity of the film material is greatly improved; the production cost of a coating conductor is reduced;the application range of the superconducting film material is expanded; wide application prospects are realized.

Description

technical field [0001] The invention belongs to the technical field of superconducting materials, and in particular relates to a high-temperature superconducting thin film material and a manufacturing method thereof. Background technique [0002] Due to its unique physical properties (zero resistance, diamagnetism, tunnel effect, etc.), superconducting materials have attracted the attention of many scientists for nearly a century. Devices and equipment such as superconducting cables, superconducting transformers, superconducting motors, superconducting current limiters, and superconducting energy storage systems made of superconducting materials have the advantages of small size, light weight, high efficiency, and energy consumption that cannot be compared with conventional products. It has the advantages of low cost and large capacity, and has broad application prospects in the field of electric power. In order to realize the application of high-temperature superconducting...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/495C04B35/622C04B35/624C04B35/632H01B12/06
CPCC04B35/495C04B35/62218C04B35/624C04B35/632C04B35/6325C04B2235/3215C04B2235/3225C04B2235/3232C04B2235/3244C04B2235/44C04B2235/449H01B12/06Y02E40/60
Inventor 蒋艳玲
Owner 蒋艳玲
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