The invention relates to a preparation method of a single domain
yttrium barium copper oxide superconductor; and the preparation method comprises the following steps: preparing Y2BaCuO5 precursor
powder and
liquid phase source
powder, pressing a Y2BaCuO5 precursor block, a
liquid phase block and a supporting bock, preparing a
green body, growing a single domain
yttrium barium copper oxide block in an infiltration manner, and carrying out
oxygen permeation processing. A second phase
nanoparticle Y2Ba4CuBiOx / Y2Ba4CuMOx (M is Bi or W) is successfully introduced for forming a
flux pinning center by adopting a top
seed crystal infiltration growing method and adding a metallic
oxide (Bi2O3
powder and WO3 powder) for
doping, thereby the powder preparation technology is simplified, the experimental period is shortened, the experiment cost is reduced, and the
flux pinning capacity of the superconductor is increased. Y2O3 is used for preparing the supporting block which stably supports two briquettes above the supporting block in the slow cold growing process of an
yttrium barium copper oxide block so as to prevent
liquid phase from running off. The preparation method can be used for preparing the
yttrium barium copper oxide superconductor and can also be used for preparing high-temperature superconductors of other series such as Gd, Sm, Nd, Eu and the like.