A montmorillonite composite flame retardant material and a preparing method thereof
A composite flame retardant and montmorillonite technology, applied in the field of montmorillonite composite flame retardant materials and their preparation, can solve the problems of producing a large amount of toxic smoke, poor flame retardant effect, unfriendly environment, etc., and achieves improved mechanical properties, enhanced Flame retardancy and mechanical properties, low cost effect
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Embodiment 1
[0028] A montmorillonite composite flame retardant material, comprising the following components by weight:
[0029] 60 parts of polypropylene resin, 1 part of modified montmorillonite, 2 parts of phosphorus-containing flame retardant, 1 part of flame retardant synergist, 1 part of compatibilizer and 0.1 part of antioxidant.
[0030] Wherein, modified montmorillonite is prepared by the following method:
[0031] Add montmorillonite to 90°C water, ultrasonically disperse for 0.5h to prepare a montmorillonite dispersion with a concentration of 5wt%, then add intercalation agent and protonating agent, control the temperature to 90°C, continue ultrasonically dispersing for 0.5h, then Filter to get the first precipitate, put the first precipitate in a beaker, add 90°C water, stir for 0.5h, filter to get the second precipitate, put the second precipitate in a beaker, add 90°C water, stir for 0.5h, Filter to obtain the third precipitate, put the third precipitate in a beaker, add 90...
Embodiment 2
[0037] A montmorillonite composite flame retardant material, comprising the following components by weight:
[0038] 80 parts of polypropylene resin, 3 parts of modified montmorillonite, 5 parts of phosphorus-containing flame retardant, 2 parts of flame retardant synergist, 5 parts of compatibilizer and 0.5 part of antioxidant.
[0039] Wherein, modified montmorillonite is prepared by the following method:
[0040] Add montmorillonite to water at 80°C, ultrasonically disperse for 1 hour to obtain a montmorillonite dispersion with a concentration of 10 wt%, then add intercalation agent and protonating agent, control the temperature at 80°C, continue ultrasonically dispersing for 1 hour, and then filter. To obtain the first precipitate, put the first precipitate in a beaker, add 80°C water, stir for 0.5h, filter to obtain the second precipitate, put the second precipitate in a beaker, add 80°C water, stir for 0.5h, filter, To obtain the third precipitate, put the third precipit...
Embodiment 3
[0046] A montmorillonite composite flame retardant material, comprising the following components by weight:
[0047] 65 parts of polypropylene resin, 1.5 parts of modified montmorillonite, 3 parts of phosphorus-containing flame retardant, 1.3 parts of flame retardant synergist, 2 parts of compatibilizer and 0.2 part of antioxidant.
[0048] Wherein, modified montmorillonite is prepared by the following method:
[0049]Add montmorillonite to water at 80°C, ultrasonically disperse for 1 hour to obtain a montmorillonite dispersion with a concentration of 6 wt%, then add intercalation agent and protonating agent, control the temperature at 80°C, continue ultrasonic dispersion for 1 hour, and then filter. To obtain the first precipitate, put the first precipitate in a beaker, add 80°C water, stir for 0.5h, filter to obtain the second precipitate, put the second precipitate in a beaker, add 80°C water, stir for 0.5h, filter, To obtain the third precipitate, put the third precipitat...
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