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Compounded hydrate anti-agglomerant and preparation method thereof

A technology of hydrate and anti-polymerization agent, which is applied in the direction of drilling compositions, chemical instruments and methods, mechanical equipment, etc., which can solve the problems of blindness in active ingredient selection and achieve good water solubility

Active Publication Date: 2018-03-09
CHINA UNIV OF PETROLEUM (BEIJING)
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  • Summary
  • Abstract
  • Description
  • Claims
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Problems solved by technology

[0005] In order to solve the above-mentioned technical problems, the purpose of the present invention is to provide a preparation method of a compound hydrate antipolymerization agent, which can solve the problems of blindness in screening active ingredients of a hydrate compound antipolymerization agent, thereby developing a A compound hydrate anti-aggregation agent obtained from plant extracts efficiently;

Method used

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  • Compounded hydrate anti-agglomerant and preparation method thereof
  • Compounded hydrate anti-agglomerant and preparation method thereof
  • Compounded hydrate anti-agglomerant and preparation method thereof

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Embodiment

[0039] This embodiment provides a preparation method of compound hydrate antipolymerization agent, which comprises the following steps:

[0040] Step 1, select the saponin tree which is one of the endemic Hemataceae Acacia tree species in my country, get the position pod with the largest biosurfactant content and grind it into 40-60 mesh powder, and heat and reflux with absolute ethanol and then filter under reduced pressure, Then use a rotary evaporator to evaporate to dryness to obtain a plant extract.

[0041] Step 2, the plant extract obtained in step 1 is segmented according to the polarity difference, and the separation schematic diagram is as follows: figure 1 As shown, the method is as follows:

[0042] Dissolve the plant extract in hot water at 70-75°C, sequentially use petroleum ether, ethyl acetate, and n-butanol for at least one extraction, combine the obtained solutions of the same phase and evaporate to dryness, and obtain the four-phase plant extract Segment: p...

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Abstract

The invention provides a compounded hydrate anti-agglomerant and a preparation method thereof. The method comprises the following steps: selecting a plant containing a biosurfaetant, extracting plantextract and segmenting the plant extract according to the polarity difference to determine an effective substance polarity segment; eluting to obtain an active part, and carrying out analysis and component deduction on the active part; compounding the deduced active ingredients to obtain the compounded hydrate anti-agglomerant. By using the preparation method of the compounded hydrate anti-agglomerant, provided by the invention, the active ingredients with an anti-agglomerating effect in the plant containing the biosurfaetant can be analyzed, detected and determined accurately and effectively,and the problems of blind screening and the like of the active ingredients of the compounded hydrate anti-agglomerant are solved. The compounded hydrate anti-agglomerant prepared by the method belongs to a plant extraction type hydrate anti-agglomerant, has the characteristics of pure nature, good water solubility, easiness in biodegradation and the like, and can be applied to hydrate anti-agglomeration of oil and gas pipelines in deep sea.

Description

technical field [0001] The invention belongs to the technical field of hydrate antipolymerization agents, and relates to a composite hydrate antipolymerization agent and a preparation method thereof. Background technique [0002] Gas hydrates are water and methane, ethane, CO 2 and H 2 Non-stoichiometric cage-like crystalline substances formed by small molecular gases such as S under low temperature and high pressure conditions. Hydrates are easily generated in natural gas / crude oil mixed pipelines to block pipelines and equipment. For a long time, oil and gas production and transportation departments have spent a lot of money on hydrate prevention and control. Today, as oil and gas resources are increasingly scarce, the focus of oil and gas development is increasingly shifting to the deep sea. The temperature and pressure conditions in the deep sea oil-gas-water three-phase mixed pipeline are very suitable for the formation of hydrates, and the problem of hydrates is part...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/524F17D1/17
CPCC09K8/524F17D1/17Y02E60/34
Inventor 王晓琴陈光进孙长宇马庆兰秦慧博刘大锰
Owner CHINA UNIV OF PETROLEUM (BEIJING)
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