A kind of composite hydrate antipolymerization agent and preparation method thereof
A technology of hydrate and anti-polymerization agent, which is applied in the direction of drilling compositions, chemical instruments and methods, mechanical equipment, etc., which can solve the problems of blindness in active ingredient selection and achieve good water solubility
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[0039] This embodiment provides a preparation method of compound hydrate antipolymerization agent, which comprises the following steps:
[0040] Step 1, select the saponin tree which is one of the endemic Hemataceae Acacia tree species in my country, get the position pod with the largest biosurfactant content and grind it into 40-60 mesh powder, and heat and reflux with absolute ethanol and then filter under reduced pressure, Then use a rotary evaporator to evaporate to dryness to obtain a plant extract.
[0041] Step 2, the plant extract obtained in step 1 is segmented according to the polarity difference, and the separation schematic diagram is as follows: figure 1 As shown, the method is as follows:
[0042] Dissolve the plant extract in hot water at 70-75°C, sequentially use petroleum ether, ethyl acetate, and n-butanol for at least one extraction, combine the obtained solutions of the same phase and evaporate to dryness, and obtain the four-phase plant extract Segment: p...
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