Solid electrolyte sheet, method for manufacturing same, and sodium ion all-solid-state secondary cell
A technology of solid electrolyte and manufacturing method, which is applied in secondary battery, electrolyte, cable/conductor manufacturing, etc., and can solve problems such as the skyrocketing price of lithium raw materials
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[0065] Hereinafter, the present invention will be described in detail based on examples, but the present invention is not limited to these examples.
[0066] Tables 1 to 3 show examples (No. 1 to 10) and comparative examples (No. 11 to 15).
[0067] [Table 1]
[0068]
[0069] [Table 2]
[0070]
[0071] [table 3]
[0072]
[0073] (a) Preparation of slurry
[0074] Sodium carbonate (Na 2 CO 3 ), sodium bicarbonate (NaHCO 3 ), magnesium oxide (MgO), aluminum oxide (Al 2 o 3 ), zirconia (ZrO 2 ), yttrium oxide (Y 2 o 3 ) to prepare the raw material powder so that it becomes the composition described in Tables 1-3. Using ethanol as the medium, the raw material powders were wet mixed for 4 hours. After evaporating ethanol, use an acrylate copolymer (OLYCOX1700 manufactured by Kyoeisha Chemical Co., Ltd.) as a binder, and use butyl benzyl phthalate as a plasticizer so that the raw material powder: binder: plasticizer = 83.5:15:1.5 (mass ratio) is weighed to d...
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