Fluoride-free waterproof finishing emulsion for textiles and application of fluoride-free waterproof finishing emulsion
A fluorine-free waterproof and emulsion technology, applied in fiber processing, textiles and papermaking, and liquid repellent fibers, etc., can solve the problem of product water resistance decline and so on
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Embodiment 1
[0067] Synthesis of component a1: Put 39g, 0.1mol of hexamethoxymethylene melamine and 162g, 0.6mol of stearyl alcohol into a 500mL four-neck flask, heat to melt the materials, then add 0.4g of concentrated hydrochloric acid, and continue to heat up to 90°C . When the system began to reflux, the methanol was evaporated under vacuum. After reacting at 90°C for 1.5h, the temperature was raised to 140°C for 2 hours. The product was a colorless and transparent viscous substance, which became a waxy solid after cooling.
Embodiment 2
[0069] Synthesis of component a2: Put 39g, 0.1mol of hexamethoxymethylene melamine and 170g, 0.6mol of octadecanoic acid into a 500mL four-neck flask, heat to melt the materials, then add 0.4g of concentrated hydrochloric acid, and continue to heat up to 90°C . When the system began to reflux, the methanol was evaporated under vacuum. After reacting at 90°C for 1.5h, the temperature was raised to 140°C for 2 hours. The product was a colorless and transparent viscous substance, which became a waxy solid after cooling.
Embodiment 3
[0071] Synthesis of component a3: Put 39g, 0.1mol of hexamethoxymethylene melamine and 188g, 0.6mol of stearyl alcohol into a 500mL four-neck flask, heat to melt the materials, then add 0.4g of concentrated hydrochloric acid, and continue to heat up to 90°C . When the system starts to reflux, add vacuum to distill methanol, and pay attention to controlling the vacuum degree to prevent material flushing. After reacting at 90°C for 1.5h, the temperature was raised to 140°C for 2 hours. The product was a light yellow transparent viscous substance, which became a waxy solid after cooling.
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