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Rotary evaporator capable of accurately achieving quantification of concentrated liquid

A technology of rotary evaporator and concentrate, applied in the direction of distillation in a rotary container, distillation separation, chemical instruments and methods, etc.

Active Publication Date: 2018-05-18
BEIJING NORMAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention provides a rotary evaporator that can accurately realize the quantitative control of concentrated liquid, and solves the problem of accurate quantitative control of concentrated liquid

Method used

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  • Rotary evaporator capable of accurately achieving quantification of concentrated liquid
  • Rotary evaporator capable of accurately achieving quantification of concentrated liquid

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Embodiment 1

[0022] see figure 1 As shown, the rotary evaporator described in this embodiment that can accurately realize the accurate quantification of concentrated liquid includes: a support 1, a detachable distillation bottle 2 and a condenser 3 are fixed on the support 1, and the distillation bottle 2 is filled with The liquid to be concentrated is heated by a heating assembly to achieve evaporation and concentration; the bottom of the condenser 3 is connected with a collection bottle 4 for collecting fractions; the support is also provided with a rotating motor 10 that controls the rotation of the distillation bottle 2 (The rotary evaporator of the present invention can also be provided with a control panel for controlling the parameter speed of the rotating motor and heating temperature, not shown in the figure), and control components for controlling the rotating speed and heating temperature.

[0023] like figure 1 In the shown rotary evaporator, the bottom of the distillation bot...

Embodiment 2

[0030] As a structure that can be transformed, such as figure 2 The structure of the rotary evaporator shown in this embodiment, the rotary evaporator that can accurately realize the quantification of the concentrated liquid described in this embodiment, includes: a support 1, a detachable distillation bottle 2 and a condenser 3 are fixed on the support 1, and the distillation The liquid to be concentrated is contained in the bottle 2, and is heated by a heating assembly to realize evaporation and concentration; the bottom of the condenser 3 is connected with a collection bottle 4 for collecting fractions; The rotary motor 10 (the rotary evaporator of the present invention can also be provided with a control panel for controlling the rotating speed, not shown in the figure), and a control assembly for controlling the heating temperature, etc.

[0031] like figure 2 In the shown rotary evaporator, the bottom of the distillation bottle 2 (based on the position of the working ...

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Abstract

The invention relates to the technical field of chemical experiment equipment, in particular to a rotary evaporator and in particular to a rotary evaporator capable of accurately achieving quantification of a concentrated liquid. According to the rotary evaporator capable of accurately achieving quantification of the concentrated liquid, a distillation bottle is improved into a structure that a liquid discharge hole is formed in the bottom, so that a concentrated liquid can be discharged on premise that the distillation bottle is not detached and the negative pressure inside a distillation system is not greatly affected; meanwhile, due to a metering tube with scales in the position of the liquid discharge hole, variations of quantities of the concentrated liquid can be visibly observed, distillation can be immediately stopped when the quantity of the concentrated liquid meets a designed accurate quantity, the precisely quantified concentrated liquid can be accurately discharged, indexes such as reaction yield can be tested, unification of detection standards can be achieved, properties of different concentrated liquids of same yield and properties of a same sample of different concentration degrees can be studied and compared.

Description

technical field [0001] The invention relates to the technical field of chemical experiment equipment, in particular to a rotary evaporator, in particular to a rotary evaporator capable of accurately quantifying concentrated liquid. Background technique [0002] Rotary evaporator is an extraction experimental equipment for vacuum distillation and concentration of materials. It is widely used in experiments such as large-scale concentration, drying, extraction and recovery of samples, especially for rapid distillation of large amounts of solvents. Existing rotary evaporators are usually composed of vacuum pumping devices, heating devices, condensing devices, rotating devices and other components. The principle of rotary evaporators is mainly controlled by electronic equipment, so that the flask rotates at a constant speed at the most suitable speed to form a thin film of solvent , increase the evaporation area, and use a vacuum pump to make the evaporation flask in a negative ...

Claims

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Application Information

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IPC IPC(8): B01D3/08B01D3/42
CPCB01D3/085B01D3/42
Inventor 温淑瑶
Owner BEIJING NORMAL UNIVERSITY
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