A kind of caulking material for colored asphalt pavement and preparation method thereof
A technology for caulking material and colored asphalt, which is applied in the field of caulking materials and their preparation, can solve the problems of gaps in the repair of colored pavement cracks, the performance of caulking materials is degraded, and the aesthetic effect is affected, so as to achieve good repair performance, stable performance, The effect of a high softening point
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Embodiment 1
[0033] Add C5 petroleum resin, C9 petroleum resin and compatibilizer into the reaction kettle, heat to 140°C to melt them all, then add the polymer and stir evenly to swell, the swelling temperature is 170°C, the time is 40min, and then pass Colloid mill with a speed of 3000 rpm once, then add coupling agent, reducing agent, anti-aging agent D (N-phenyl-2-naphthylamine) and stir for 30 minutes, and then pass through a colloid mill with a speed of 3000 rpm 2 times, then add vulcanizing agent and stir in the product tank at 170°C for 8 hours to obtain the caulking material. The name, specification model and proportioning ratio of each raw material of this embodiment are shown in Table 1 below, and the properties of the products obtained are shown in Table 6.
[0034] Table 1 Raw material name, ratio and type of caulking material
[0035] Raw material category specific name Specifications Quality score, % Petroleum resin 1 C5 Chroma 6 1 Petroleum res...
Embodiment 2
[0037] Add petroleum resin and compatibilizer into the reaction kettle, heat it to 125°C to melt it completely, then add polymer and stir evenly, then swell. Minute colloid mill once, then add coupling agent, reducing agent, anti-aging agent RD (2,2,4-trimethyl-1,2-dihydroquinoline polymer) and stir for 60 minutes, passing through at a speed of 3000 rpm Colloid mill 2 times per minute, then add vulcanizing agent and stir in a product tank at 175°C for 8 hours to obtain the caulking material. The name, specification model and proportioning ratio of each raw material of this embodiment are shown in Table 2 below, and the properties of the product obtained are shown in Table 6.
[0038] Table 2 Raw material names, ratios and types of caulking materials
[0039] Raw material category specific name Specifications Quality score, % Petroleum resin 1 C5 Chroma 6 10 Petroleum resin 2 C9 Chroma 15 5 Compatibilizer rubber filling oil Viscosity 30...
Embodiment 3
[0041] Add petroleum resin and compatibilizer into the reaction kettle, heat to 130°C to melt them all, then add polymer and stir evenly, then swell. 1 minute colloid mill 1 time, then add coupling agent, reducing agent, anti-aging agent and stir evenly, pass the colloid mill 2 times that the rotating speed is 3000 rev / min after the reaction finishes, add vulcanizing agent 1 and vulcanizing agent 2 afterwards, at 170 Stir in the product tank at ℃ for 8 hours to obtain the caulking material. The name, specification model and proportioning ratio of each raw material of this embodiment are shown in Table 3 below, and the properties of the products obtained are shown in Table 6.
[0042] Table 3 Raw material names, ratios and types of caulking materials
[0043] Raw material category specific name Specifications Quality score, % Petroleum resin 1 C5 Chroma 19 5 Petroleum resin 2 C9 Chroma 7 7 Compatibilizer Refined Aromatic Oil Viscosity a...
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