Nonaqueous lithium storage element
A technology for electric storage components and non-aqueous electrolytes, which is applied to electrical components, non-aqueous electrolyte batteries, lithium batteries, etc., and can solve problems such as unconsidered suppression, resistance rise, and energy density reduction
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[0270] The preparation of the above-mentioned coating solution for the positive electrode precursor is not particularly limited, and a disperser such as a homogeneous disperser, a multi-shaft disperser, a planetary mixer, a thin film rotary high-speed mixer, etc. can be suitably used. In order to obtain a coating liquid in a good dispersion state, it is preferable to disperse at a peripheral speed of 1 m / s to 50 m / s. When the peripheral speed is 1 m / s or more, various materials can be dissolved or dispersed well, which is preferable. In addition, when the peripheral speed is 50 m / s or less, various materials are not broken by heat or shear force generated by dispersion, and re-agglomeration does not occur, so it is preferable.
[0271] Regarding the degree of dispersion of the coating liquid, the particle size measured by a particle size meter is preferably 0.1 μm or more and 100 μm or less. As the upper limit of the degree of dispersion, the particle size is more preferably ...
Embodiment 1
[0553]
preparation example 1a
[0555] The crushed coconut shell carbides were carbonized in a small carbonization furnace at 500°C for 3 hours in nitrogen to obtain carbides. Put the obtained carbide into the activation furnace, introduce 1 kg / h of water vapor into the activation furnace in the state of being heated by the preheating furnace, and heat up to 900° C. for 8 hours for activation. The activated carbide was taken out and cooled under a nitrogen atmosphere to obtain activated activated carbon. The obtained activated carbon was washed with water for 12 hours, and then water was removed. Thereafter, it was dried in an electric dryer maintained at 125°C for 10 hours, and then pulverized by a ball mill for 1 hour to obtain activated carbon 1a.
[0556] The average particle diameter of this activated carbon 1a was 12.7 μm when measured using a laser diffraction particle size distribution analyzer (SALD-2000J) manufactured by Shimadzu Corporation. In addition, the pore distribution was measured using ...
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