Admixture for inhibiting bleeding of fabricated concrete and preparation method of admixture
An admixture and concrete technology, which is applied in the field of admixtures and its preparation for inhibiting prefabricated concrete bleeding, can solve the problems of affecting the appearance quality of concrete, large adverse effects, and weakening the surface appearance quality of concrete components, so as to ensure the appearance quality, High adaptability, the effect of avoiding delayed bleeding
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Embodiment 1
[0042] A kind of preparation method of polycarboxylate water reducing component comprises the steps:
[0043] 1) Dissolve 160 g of allyl polyoxyethylene ether with a molecular weight of 3500 in 100 g of water to form solution A;
[0044] 2) Dissolve 13g of acrylic acid and 3.3g of N-(3-dimethylaminopropyl)methacrylamide in 8g of water to prepare solution B;
[0045] 3) Dissolve 0.6g of mercaptopropionic acid and 0.3g of L-ascorbic acid in 45g of water to form solution C;
[0046] 4) Heat solution A to 50°C, add 0.45g of hydrogen peroxide to A, then add solutions B and C to A at the same time, the dropping time of solution B is 3.0h, and the dropping time of solution C 3.5h;
[0047] After all the addition is completed, continue to react for 1 hour, then reduce the temperature of the reaction solution to room temperature, adjust the pH value of the reaction solution to 6.0 with 20 g of sodium hydroxide solution (30 wt %), then add 109 g of water to obtain a mass concentration...
Embodiment 2
[0051] A kind of preparation method of polycarboxylate water reducing component comprises the steps:
[0052] 1) Dissolve 182 g of allyl polyoxyethylene ether with a molecular weight of 4000 in 120 g of water to form solution A;
[0053] 2) Dissolve 13g of acrylic acid and 3.3g of N-(3-dimethylaminopropyl)methacrylamide in 8g of water to prepare solution B;
[0054] 3) Dissolve 0.6g of mercaptopropionic acid and 0.3g of L-ascorbic acid in 45g of water to form solution C;
[0055] 4) Heat solution A to 50°C, add 0.45g of hydrogen peroxide to A, then add solutions B and C to A at the same time, the dropping time of solution B is 3.0h, and the dropping time of solution C 3.5h;
[0056] After all the addition is completed, continue to react for 1 hour, then reduce the temperature of the reaction solution to room temperature, adjust the pH value of the reaction solution to 6.0 with 20 g of sodium hydroxide solution (30 wt %), then add 122 g of water to obtain a mass concentration...
Embodiment 3
[0060] A kind of preparation method of polycarboxylate water reducing component comprises the steps:
[0061] 1) Dissolve 182 g of allyl polyoxyethylene ether with a molecular weight of 4000 in 120 g of water to form solution A;
[0062] 2) Dissolve 13g of acrylic acid and 5.0g of N-(3-dimethylaminopropyl)methacrylamide in 10g of water to form solution B;
[0063] 3) Dissolve 0.6g of mercaptopropionic acid and 0.3g of L-ascorbic acid in 45g of water to form solution C;
[0064] 4) Heat solution A to 50°C, add 0.45g of hydrogen peroxide to A, then add solutions B and C to A at the same time, the dropping time of solution B is 3.0h, and the dropping time of solution C 3.5h;
[0065] After all the addition is completed, continue to react for 1 hour, then reduce the temperature of the reaction solution to room temperature, adjust the pH value of the reaction solution to 6.0 with 20 g of sodium hydroxide solution (30 wt %), then add 122 g of water to obtain a mass concentration o...
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