A kind of concrete anti-crack reinforcement additive and preparation method thereof
An additive and concrete technology, which is applied in the field of construction, can solve problems such as easy cracks, high brittleness, and impact, and achieve high tensile strength and compressive strength, good crack resistance and impermeability, and is conducive to industrial production.
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Embodiment 1
[0025] A concrete anti-cracking reinforcing additive, comprising the following raw materials in parts by weight: 16 parts of chitosan, 15 parts of sodium 4-cumenesulfonate, 12 parts of 2-mercaptobenzothiazole, and methyl dihydrojasmonate 6 parts, 11 parts of p-nitrosoxylene and 7 parts of isooctyl acetate.
[0026] A method for preparing concrete anti-cracking reinforcing additives, the specific steps are: (1) adding p-nitrosoxylene, chitosan and methyl dihydrojasmonate into a reaction kettle, and adding 20 parts of 85% Ethanol solution, protected by nitrogen, placed at -70°C and stirred for 2 hours; (2) Mix 2-mercaptobenzothiazole and isooctyl acetate, add 75% ethanol solution of 2 times the weight of the mixture, and mix well; Liquid one; (3) Add the mixed liquid dropwise to the reaction kettle of step (1), the dropping rate is 100 drops / min; (4) The reaction kettle is heated to -5°C, and sodium 4-cumenesulfonate is added, Stir the reaction for 1 hour; (5) continue to heat up ...
Embodiment 2
[0028] A concrete anti-cracking reinforcement additive, comprising the following raw materials in parts by weight: 32 parts of chitosan, 22 parts of sodium 4-cumenesulfonate, 19 parts of 2-mercaptobenzothiazole, methyl dihydrojasmonate 17 parts, 17 parts p-nitrosoxylene amine, 15 parts isooctyl acetate.
[0029] A method for preparing concrete anti-cracking reinforcing additives, the specific steps are: (1) adding p-nitrosoxylene, chitosan and methyl dihydrojasmonate into a reaction kettle, and adding 35 parts of 85% Ethanol solution, protected by nitrogen, placed at -70℃ and stirred for 3h; (2) Mix 2-mercaptobenzothiazole and isooctyl acetate, add 4 times the weight of the 75% ethanol solution to the mixture, and mix well; Liquid one; (3) Add the mixed liquid one drop to the reaction kettle of step (1), the dropping rate is 200 drops / min; (4) The reaction kettle is heated to -5°C, and sodium 4-cumenesulfonate is added, Stir and react for 3h; (5) continue to heat the resultant f...
Embodiment 3
[0031] A concrete anti-cracking reinforcing additive, comprising the following raw materials in parts by weight: 25 parts of chitosan, 17 parts of sodium 4-cumenesulfonate, 15 parts of 2-mercaptobenzothiazole, and methyl dihydrojasmonate 11 parts, 13 parts p-nitrosoxylene, 11 parts isooctyl acetate.
[0032] A method for preparing a concrete anti-cracking reinforcing additive. The specific steps are as follows: (1) Add p-nitrosoxylene, chitosan and methyl dihydrojasmonate to a reaction kettle, and add 25 parts of 85% Ethanol solution, protected by nitrogen, placed at -70°C and stirred for 2.5h. (2) Mixing 2-mercaptobenzothiazole and isooctyl acetate, adding a 75% ethanol solution of 2.4 times the weight of the mixture, and mixing uniformly; a mixed solution one is obtained. (3) Add the mixed liquid to the reaction kettle of step (1) one drop at a rate of 150 drops / min. (4) The reaction kettle was heated to -5°C, sodium 4-cumenesulfonate was added, and the reaction was stirred f...
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