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Method for improving function stability of nickel-titanium shape memory alloy

A technology of memory alloy and stability, which is applied in the field of nickel-titanium shape memory alloy, can solve problems such as the insignificant strength effect of the nickel-titanium shape memory alloy matrix, difficulty in handling nickel-titanium alloy components, and unsuitable nickel-titanium alloy components, etc., to achieve improvement Functional stability, improvement of matrix strength, and effect of improving functional stability

Active Publication Date: 2018-11-06
SHANDONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the use of severe plastic deformation and post-treatment to refine the structure of nickel-titanium shape memory alloy mainly has the following disadvantages: (1) Due to the characteristics of high strength and strong work hardening ability of nickel-titanium shape memory alloy, it needs to be processed at a higher temperature. Severe plastic deformation process, which will seriously limit the effect of grain refinement, and it is difficult to obtain a grain structure below 100nm; (2) The severe plastic deformation process is only suitable for samples with simple shapes (such as plates, rods, pipes, etc.) etc.), it is difficult to handle nickel-titanium alloy components with complex structures
However, at present, the method of simply using aging strengthening or grain refinement to improve the strength of the nickel-titanium shape memory alloy matrix has no obvious effect, and is not suitable for processing nickel-titanium alloy components with complex structures.

Method used

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  • Method for improving function stability of nickel-titanium shape memory alloy
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  • Method for improving function stability of nickel-titanium shape memory alloy

Examples

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Embodiment 1

[0037] A method for improving the functional stability of a nickel-titanium shape memory alloy, comprising the steps of: first, stretching and deforming the nickel-titanium shape memory alloy to 9.5% at room temperature, then unloading, and repeating the above process 10 times, the nickel-titanium shape memory alloy Introducing dislocation defects; then aging for 48 hours under the condition of 250° C., introducing nanometer two-phase particles into the nickel-titanium shape memory alloy to obtain.

[0038] The atomic percentage of nickel in the nickel-titanium shape memory alloy used in this embodiment is 50.8 at.%.

Embodiment 2

[0040] A method for improving the functional stability of a nickel-titanium shape memory alloy, comprising the following steps: first, keeping the nickel-titanium shape memory alloy in a water bath at 100° C. for 5 minutes, then putting it into liquid nitrogen for 5 minutes, and then putting it into the Keep warm in a water bath at 100°C for 5 minutes, repeat the above process 20 times, and introduce dislocation defects into the nickel-titanium shape memory alloy; then age at 250°C for 48 hours, and introduce nano-secondary phase particles into the nickel-titanium shape memory alloy, that is, .

[0041] The atomic percentage of nickel in the nickel-titanium shape memory alloy used in this embodiment is 50.8 at.%.

Embodiment 3

[0043] A method for improving the functional stability of a nickel-titanium shape memory alloy, comprising the following steps: first, keeping the nickel-titanium shape memory alloy in a water bath at 100° C. for 5 minutes, then putting it into liquid nitrogen for 5 minutes, and then putting it into the Keep warm in a water bath at 100°C for 5 minutes, repeat the above process 200 times, and introduce dislocation defects into the nickel-titanium shape memory alloy; then age at 150°C for 500 hours, and introduce nanometer two-phase particles into the nickel-titanium shape memory alloy. .

[0044] The atomic percentage of nickel in the nickel-titanium shape memory alloy used in this embodiment is 50 at.%.

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Abstract

The invention relates to a method for improving the function stability of a nickel-titanium shape memory alloy, and belongs to the field of nickel-titanium shape memory alloys. According to the method, dislocations and other defects are introduced into the nickel-titanium shape memory alloy, the dislocations serve as activity position points for promoting second phase nucleation, then, fine and evenly-distributed nano reinforcement phases are formed in a matrix structure of the nickel-titanium shape memory alloy through later aging treatment, accordingly, the matrix strength of the nickel-titanium shape memory alloy is obviously improved, and then the function stability of the alloy is improved. Meanwhile, in the method, only temperature martensite phase change induction circulation or stress martensite phase change induction circulation need to be conducted on a nickel-titanium shape memory alloy component before aging treatment, and operation is simple and convenient; and the methoddoes not have the requirement for the shape of the nickel-titanium shape memory alloy component, and the method is adaptive to the complex nickel-titanium shape memory alloy component and capable of effectively improving the function stability of the complex nickel-titanium shape memory alloy component.

Description

technical field [0001] The invention belongs to the field of nickel-titanium shape memory alloys, and in particular relates to a method for improving the functional stability of nickel-titanium shape memory alloys through the synergistic effect of cyclic loading and low-temperature aging. Background technique [0002] Nickel-titanium shape memory alloy exhibits shape memory effect and superelasticity, and is an intelligent material integrating sensing and driving. It has broad application prospects in the automotive industry, artificial intelligence, aerospace, marine transportation, and biomedical fields. Nickel-titanium shape memory alloy components generally undergo repeated phase transformation processes in practical applications. In this process, the accumulation of plastic deformation caused by cyclic phase transformation is the main reason for the decrease in the functional stability of nickel-titanium shape memory alloy components. . This severely limits the servic...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C19/03C22F1/10
CPCC22C19/03C22C2202/00C22F1/006C22F1/10
Inventor 王协彬蒲泽王作成
Owner SHANDONG UNIV
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