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Preparation method of novel antibacterial agent

An antibacterial agent, a certain amount of technology, applied in the field of preparation of new antibacterial agents

Inactive Publication Date: 2019-01-08
ANHUI JIANGHUAI AUTOMOBILE GRP CORP LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This antibacterial agent has not been reported so far, which has very important practical significance for expanding the types and applications of antibacterial agents

Method used

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  • Preparation method of novel antibacterial agent
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  • Preparation method of novel antibacterial agent

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preparation example Construction

[0021] The application provides a preparation method of an antibacterial agent, comprising the following steps:

[0022] (1) Weigh a certain amount of diyttrium trioxide, deionized water, and nitric acid, add them to the reaction vessel, and react at 40-60°C for 3-5h to form Y(NO3) 3 ·6H 2 O; the mass ratio of diyttrium trioxide, deionized water, and nitric acid is (20-30): (120-160): (50-70).

[0023] (2) Weigh a certain amount of nonylphenol polyoxyethylene ether, glycerol, cycloheptane, Y(NO3) 3 ·6H 2 O, add them to the reaction vessel, stir and react at room temperature for 2-4h to form solution A; nonylphenol polyoxyethylene ether, glycerol, cycloheptane, Y(NO3) 3 ·6H 2 The mass ratio of O is (3-7):(8-10):(30-50):(80-100).

[0024] (3) Weigh a certain amount of nonylphenol polyoxyethylene ether, glycerol, cycloheptane, 5-chloro-7-hydroxyquinoline, and sodium o-hydroxyphenylacetate, and add them to the reaction vessel. Under stirring reaction 1-3h, form solution B; T...

Embodiment 1

[0028] (1) Weigh 200g of diyttrium trioxide, 1.2kg of deionized water, and 500g of nitric acid, add them to the reaction vessel, and react at 40°C for 3 hours to form Y(NO3) 3 ·6H 2 O.

[0029] (2) Weigh 30g nonylphenol polyoxyethylene ether, 80g glycerin, 300g cycloheptane, 800gY(NO3) 3 ·6H 2 O, they were added to the reaction vessel, stirred and reacted at room temperature for 2h to form solution A.

[0030] (3) Weigh 40g nonylphenol polyoxyethylene ether, 60g glycerol, 200g cycloheptane, 10g5-chloro-7-hydroxyquinoline, 500g sodium o-hydroxyphenylacetate, add them to the reaction vessel, and The reaction was stirred at room temperature for 1 h to form solution B.

[0031] (4) Weigh 400g of solution A, 300g of solution B, and 100g of tetraethyl orthosilicate, add them to the reaction vessel, stir and react at room temperature for 3h, centrifuge with a centrifuge, draw the clear liquid, and then use Wash with ethanol and distilled water, centrifuge twice, place in an oven...

Embodiment 2

[0041] (1) Weigh 300g of diyttrium trioxide, 1.6kg of deionized water, and 700g of nitric acid, add them to the reaction vessel, and react at 60°C for 5h to form Y(NO3) 3 ·6H 2 O.

[0042] (2) Weigh 70g nonylphenol polyoxyethylene ether, 100g glycerol, 500g cycloheptane, 1.0kgY(NO3) 3 ·6H 2 O, they were added to the reaction vessel, stirred and reacted at room temperature for 4h to form solution A.

[0043] (3) Weigh 60g nonylphenol polyoxyethylene ether, 100g glycerol, 300g cycloheptane, 30g 5-chloro-7-hydroxyquinoline, 700g sodium o-hydroxyphenylacetate, add them to the reaction vessel, and The reaction was stirred at room temperature for 3 h to form solution B.

[0044] (4) Weigh 600g of solution A, 500g of solution B, and 200g of tetraethylorthosilicate, add them to the reaction vessel, stir and react at room temperature for 5h, centrifuge with a centrifuge, draw the clear liquid, and use Wash with ethanol and deionized water, centrifuge twice, put in an oven at 100°C...

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Abstract

The invention relates to a preparation method of a novel antibacterial agent. A certain amount of yttria, a certain amount of deionized water and a certain amount of nitric acid are weighed, and Y(NO3)3*6H2O is formed; a certain amount of nonylphenol polyoxyethylene ether, a certain amount of glycerin, a certain amount of cycloheptane and a certain amount of Y(NO3)3*6H2O are weighed, and a solution A is formed; a certain amount of nonylphenol polyoxyethylene ether, a certain amount of glycerin, a certain amount of cycloheptane, a certain amount of 5- chloro-7-hydroxyquinoline and a certain amount of sodium o-hydroxyphenylacetate are weighed, and a solution B is formed; a certain amount of the solution A, a certain amount of the solution B and a certain amount of tetraethoxysilane are weighed, and the antibacterial agent is obtained. According to the technical scheme, the antibacterial performance of a polyolefin composite is improved through addition of the specially-made antibacterialagent, and the antibacterial agent has the great promotional value.

Description

technical field [0001] The invention belongs to the technical field of polymer materials, in particular to a preparation method of a novel antibacterial agent. Background technique [0002] In order to effectively prevent the pollution and infringement of bacteria and other microorganisms, the use of antibacterial materials has become an urgent need and choice. Antibacterial agents are the most critical part of antibacterial materials in their antibacterial effect. This technical solution innovatively synthesizes a new type of antibacterial agent, which can well improve the antibacterial performance of polyolefin composite materials. This antibacterial agent has not been reported so far, which has very important practical significance for expanding the types and applications of antibacterial agents. Contents of the invention [0003] The purpose of the present invention is to provide a preparation method of a novel antibacterial agent, and the prepared antibacterial agent...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/12C08L67/02C08L23/06C08L77/02C08L25/06C08L71/02C08K13/02C08K3/28C08K5/3437C08K5/136C08K5/5415
Inventor 刘凯孙启林李凡
Owner ANHUI JIANGHUAI AUTOMOBILE GRP CORP LTD
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