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Continuous flow production control method, device and system for microreactor

A production control method and micro-reactor technology, applied in control/regulation systems, chemical instruments and methods, chemical/physical/physicochemical reactors, etc., capable of solving reaction product fluctuations, unstable output products, lack of detection and regulation Control methods and other issues to achieve the effect of ensuring stable output and realizing real-time analysis and control

Inactive Publication Date: 2019-01-15
鸿微(昆山)工程技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, for some production processes with relatively harsh reaction conditions, small changes in input conditions (such as flow, temperature, pressure fluctuations, etc.) fluctuate and cause instability of the output product
[0004] At present, the control of the microreactor system is often the monitoring and control of the flow, temperature, pressure and other inputs. In the case of continuous flow production operations, there is still a lack of detection and adjustment control means for product analysis and changes.

Method used

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  • Continuous flow production control method, device and system for microreactor
  • Continuous flow production control method, device and system for microreactor
  • Continuous flow production control method, device and system for microreactor

Examples

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Embodiment 1

[0057] figure 1 It is a flow chart of a continuous flow production control method for a microreactor provided in an embodiment of the present invention, such as figure 1 As shown, the method in this embodiment may specifically include the following steps:

[0058] S101. Detect the components of the reaction raw materials and the component content data corresponding to each of the components;

[0059] Raw materials refer to raw materials that need to be reacted in chemical production, including liquid raw materials, solid raw materials, and gas raw materials. The reaction can be liquid and liquid reaction, liquid and solid reaction, or gas raw material and liquid raw material reaction. For the reaction of solid and liquid, the solid raw material is made into particles below 200 microns and then uniformly dispersed and suspended in the liquid phase and input into the reaction system. For the gas and liquid reaction, the interface of the gas and liquid mixing interface is spec...

Embodiment 2

[0084] figure 2 It is a structural schematic diagram of a microreactor continuous flow production control device provided by the embodiment of the present invention. Such as figure 2 Shown, a kind of continuous flow production control device of microreactor comprises:

[0085] The detection module 201 is used to detect the components of the reaction raw materials and the component content data corresponding to each of the components;

[0086] The simulation module 202 is used to simulate the reaction process, and determine the simulated reaction product in the simulated reaction process;

[0087] An analysis module 203, configured to analyze the component data of the simulated reaction product and the simulated component content data corresponding to the components of the simulated reaction product, to determine the first analysis data;

[0088] The collection module 204 is used to collect the component data of the actual reaction product sample and the content data corre...

Embodiment 3

[0097] image 3 It is a structural schematic diagram of a microreactor continuous flow production control system. Such as image 3 As shown, a continuous flow production control system for a microreactor includes:

[0098] Control module 301, raw material input module 302, online mass spectrometer 303, microreactor module 304, microfluidic chip 305, product collection device 306;

[0099] The raw material input module communication end of the control module 301 is connected to the communication end of the raw material input module 302, and is used to detect the components of the reaction raw materials of the raw material input module 302 and the component content data corresponding to each of the components;

[0100] Optionally, the control module 301 can adopt an industrial control computer, and the simulation calculation model program is written in the industrial control computer, and has at least two communication terminals, which are respectively the communication termin...

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Abstract

The invention relates to a continuous flow production control method, device and system for a microreactor. The method includes the steps: detecting the components of reaction raw materials and the corresponding component content data of all the components; simulating a reaction process, and determining simulated reaction products; analyzing the component data of the simulated reaction products and the corresponding simulated component content data of the simulated reaction product components, and determining first analysis data; collecting the component data of real reaction products and thecorresponding content data of the real reaction product components, and determining second analysis data; carrying out comparative analysis of the first analysis data with the second analysis data, and determining first comparative analysis result data; and if the first analysis data and the second analysis data are changed, adjusting the reaction conditions and / or reaction raw material proportionaccording to the first comparative analysis result data, determining a control scheme and controlling the microreactor to produce the target product. The method or device or system can monitor and analyze the reaction process in real time and adjust the reaction raw material proportion and / or reaction conditions in real time.

Description

technical field [0001] The invention relates to the application field of microchemical technology, in particular to a continuous flow production control method, device and system of a microreactor. Background technique [0002] In recent years, microreactor technology, as an important technical means of chemical process intensification, has gradually become a hot spot in research and application. Around the core process of "three transmissions and one inversion" in chemical production, relying on the large reduction of characteristic size, microreactors are in the process of mass transfer. , heat transfer and other processes, the efficiency is increased by 10 to 100 times compared with conventional equipment. For some rapid reaction processes, microreactors have many advantages such as good safety, process controllability and direct scale-up. [0003] At present, for the reaction process controlled by heat and mass transfer, it is a main direction of the application of micr...

Claims

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Application Information

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IPC IPC(8): B01J19/00G05D27/02G01N27/62
CPCB01J19/0006B01J19/0093G05D27/02G01N27/62B01J2219/00049
Inventor 彭强钱文海
Owner 鸿微(昆山)工程技术有限公司
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