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A quality detection method for concentrated Huoxin pills

A quality inspection method and technology for Huoxin Pills, which can be applied to measurement devices, instruments, scientific instruments, etc., and can solve the problems of insufficient comprehensiveness and one-sidedness of concentrated Huoxin Pills.

Active Publication Date: 2021-04-27
GUANGZHOU RUIKANG BIOLOGICAL PHARMA
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Problems solved by technology

[0008] The purpose of the present invention is to provide a quality detection method for concentrated Huoxin pills, which solves the problem of one-sidedness and insufficient comprehensiveness in the existing quality standard detection of concentrated Huoxin pills, and realizes comprehensive and effective control of the quality of the product

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  • A quality detection method for concentrated Huoxin pills
  • A quality detection method for concentrated Huoxin pills
  • A quality detection method for concentrated Huoxin pills

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Embodiment Construction

[0044] The quality detection method of described concentrated heart pill comprises following identification method and assay method:

[0045] (1) Identification method

[0046] 1. TLC identification of muscone

[0047] ①Materials and reagents: Merck silica gel G thin-layer plates. All other reagents were analytically pure.

[0048] ②Reference substance: Muscone reference substance, batch number 110719-201014, purchased from China Inspection Institute.

[0049] ③ Test product: Concentrated Huoxin Pills with batch numbers 12030201, 12050101, 12060101, 12070101, 12080101, provided by Guangzhou Yuekang Biopharmaceutical Co., Ltd.

[0050] Take 0.8g each of 5 batches of the test sample, grind it finely, add 15ml of ether, ultrasonic treatment for 15 minutes, filter, filter the residue for later use, evaporate the filtrate, add 1ml of ethanol to the residue to dissolve, and use it as the test solution; For the reference substance, add ethanol to make a solution containing 1mg pe...

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Abstract

The invention provides a quality detection method of concentrated Huoxin pills, the quality detection method of said concentrated Huoxin pills includes the identification and content determination of the following active ingredients, identification: first take the concentrated Huoxin pills to make the test solution, and then take another Muscone, borneol, toad venom, bear bile, and ginseng reference substances were prepared as reference substance solutions, and then tested according to thin-layer chromatography. In the chromatogram of the test substance, on the position corresponding to the chromatogram of the reference substance, fluorescent spots of the same color were displayed; Determination of content: According to the determination by high performance liquid chromatography, the concentrated Huoxin pills contain in vitro cultured bezoar per 1 g, calculated as bilirubin, not less than 5.5 mg; The total amount of borneol must not be less than 1.8 mg; according to gas chromatography, the concentrated Huoxin pills contain artificial musk per 1 g, calculated as muscone, and must not be less than 1.0 mg; per 1 g contains borneol and borneol The total amount shall not be less than 13.5mg.

Description

technical field [0001] The invention belongs to the field of drug testing, in particular to a quality testing method for concentrated Huoxin pills. Background technique [0002] Huoxin Pill is a 2010 national drug standard improvement product, produced by Guangzhou Yuekang Biopharmaceutical Co., Ltd. [0003] Concentrated Huoxin Pills have the effects of nourishing qi and activating blood circulation, warming the meridians and dredging the meridians. Indications of chest obstruction, heart pain, suitable for coronary heart disease, angina pectoris. [0004] Concentrated Huoxin Pills are black or golden-yellow coated concentrated water pills, brown to dark brown after removing the coating; fragrant, pungent and numb. [0005] The prescription is: Ganoderma lucidum 20g, artificial musk 1.2g, bear bile 2.4g, in vitro cultured bezoar 1.2g, pearl 2.4g, ginseng 18g, toad venom 1.8g, aconite (Heishun slice) 9g, borneol 1.2g, safflower 2.0g. [0006] The preparation method is: th...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/02G01N30/06
CPCG01N30/02G01N30/06
Inventor 上官康
Owner GUANGZHOU RUIKANG BIOLOGICAL PHARMA
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