Testing method for Xueshuan xinmaining tablet

A technology for the detection of blood clots and heart pulses, which is applied in the direction of measuring devices, instruments, scientific instruments, etc., can solve the problems of divided operations, incompleteness, and low specificity of detection methods, etc., to achieve strong specificity and easy operation Effect

Active Publication Date: 2013-10-16
吉林华康药业股份有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The present invention provides a detection method for Xueshuan Xinmaining Tablets to solve the problems of weak specificity, divided operation and incompleteness existing in the current detection method

Method used

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  • Testing method for Xueshuan xinmaining tablet
  • Testing method for Xueshuan xinmaining tablet
  • Testing method for Xueshuan xinmaining tablet

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Including the following identification methods and content determination methods:

[0030] (1) Identification method

[0031] (1) Take 20 tablets of this product, grind them finely, add 40ml of diethyl ether to cold soak for 1 hour, filter, evaporate the filtrate to dryness, add 2ml of absolute ethanol to dissolve the residue, and use it as the test solution; Chuanxiong reference drug 1g, the same method as the reference drug solution; then take tanshinone IIA reference substance, borneol reference substance, add ethyl acetate to make a solution containing 1mg per 1ml, as the reference solution; test according to thin-layer chromatography, absorb the above 1 μl of each of the five solutions was spotted on the same silica gel G thin-layer plate, developed with petroleum ether 60-90°C-ethyl acetate 11:2 as the developing solvent, taken out, and dried in the air; At the positions corresponding to the chromatograms of the Danshen reference medicinal material and Tanshinone...

Embodiment 2

[0045] The identification method is the same as in Example 1.

[0046] In the content determination method, the preparation of the test solution in the content determination of Rhizoma Chuanxiong: take 20 pieces of this product, accurately weigh, grind finely, get 0.3g, accurately weigh, and the rest are the same as in Example 1.

[0047] Preparation of test solution in the determination of ginseng stem and leaf saponin content: take 20 pieces of this product, accurately weighed, grind finely, get 0.4g, accurately weigh, and the rest are the same as in Example 1.

Embodiment 3

[0049] The identification method is the same as in Example 1.

[0050] In the content determination method, the preparation of the test solution in the content determination of Rhizoma Chuanxiong: take 20 pieces of this product, accurately weigh, grind finely, get 0.4g, accurately weigh, and the rest are the same as in Example 1.

[0051] Preparation of the test solution in the determination of saponins in ginseng stems and leaves: take 20 pieces of this product, accurately weigh, grind finely, get 0.6g, accurately weigh, and the rest are the same as in Example 1.

[0052] Each tablet of this product contains chuanxiong and ferulic acid (C 10 h 10 o 4 ), not less than 0.10mg.

[0053] Each tablet of this product contains ginseng stem and leaf saponins and ginsenoside Rg1 (C 42 h 72 o 14 ) and ginsenoside Re(C 48 h 82 o 18 ) in total, not less than 4.0 mg.

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Abstract

The invention relates to a testing method for a Xueshuan xinmaining tablet, and belongs to the field of traditional Chinese medicine testing. The method comprises steps of identification of a red sage root, a rhizoma ligustici wallichii, and borneol through spreading a sample on a thin layer system, gas chromatography identification of artificial musk, thin layer identification of calculus bovis factitious, and content determination of the rhizoma ligustici wallichii and saponin in stems and leaves of a ginseng, and has the characteristics of good specialization, fastness, economy, convenience in operation and the like; meanwhile, the identification of calculus bovis factitious and artificial musk is added; the method establishes the multi-index content determination; particularly through the content determination of rhizoma ligustici wallichii and saponin in the stems and the leaves of the ginseng , and the combination with the original content determination, the components of a drug can be tested more comprehensively, the content and the reliability of the monarch drug can be recognized, and the explanation of material base for drug taking is facilitated.

Description

technical field [0001] The invention belongs to the field of traditional Chinese medicine modernization, and in particular relates to a detection method for Xueshuan Xinmaining Tablets. Background technique [0002] The composition of traditional Chinese medicine is complex, especially the compound prescription of traditional Chinese medicine often contains many kinds and many kinds of ingredients, forming a very complicated system. At present, the research and development of new effective parts of traditional Chinese medicine preparations and modern compound Chinese medicine preparations are increasing, and new processes and various extraction methods are used in the research and production of medicines. [0003] With the rapid development of modern analysis and testing technology, equipment and instruments, the content determination and chromatographic identification of traditional Chinese medicine have become important means of detection. However, at present, only the co...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90G01N30/88
Inventor 丁桂兰洪梅刘艳秋商慧娟夏宝森
Owner 吉林华康药业股份有限公司
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