Mouth wash containing cannabinoid and preparing method of mouth wash
Mouthwash and cannabinoid technology, applied in the field of cannabinoid-containing mouthwash and its preparation, can solve the problems of unreported ratio of active ingredients, undisclosed oral bacteria inhibitory effect, etc., to maintain oral health, simple preparation method, maintain breath freshening effect
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Embodiment 1
[0059] The preparation of embodiment 1 cannabinoid
[0060] 1. Experimental steps
[0061] (1) Grinding industrial hemp flower and leaf raw materials into 60-mesh coarse powder, baking at 140°C for 60 minutes, and moisture is 3.2%;
[0062] (2) soak the medicinal material obtained in step (1) with 10 times of 80% ethanol at room temperature for 3 hours, extract 3 times, and combine to obtain the extract;
[0063] (3) Concentrate the extract obtained in step (2) at 65°C to a paste concentrate (relative density 1.08, measured at 50°C);
[0064] (4) Extract the paste-like concentrated solution obtained in step (3) with 3 times the amount of medicinal materials and n-hexane for 3 times, stir for 1 hour, take the upper layer after layering, combine the upper layer, and concentrate at 65°C to a thick paste (relative density 1.08, measured at 50°C);
[0065] (5) Add sodium hydroxide to the thick paste obtained in step (4) to adjust the pH to 11, fully stir for 1 h, filter, then ad...
Embodiment 2
[0086] The preparation of embodiment 2 cannabinoids
[0087] (1) Grinding industrial hemp flower and leaf raw materials into 60-mesh coarse powder, baking at 150°C for 80 minutes, and the moisture is 2.1%;
[0088] (2) soak the medicinal material obtained in step (1) with 15 times of 95% ethanol at room temperature for 6 hours, and extract 5 times;
[0089] (3) Concentrate the extract obtained in step (2) at 65°C to a paste concentrate (relative density 1.08, measured at 50°C);
[0090] (4) Extract the paste-like concentrated liquid obtained in step (3) with 5 times the amount of medicinal material with n-hexane for 4 times, stir for 1 hour, take the upper layer after layering, concentrate at 65°C to a thick paste (relative density 1.08, measured at 50°C have to);
[0091] (5) Add sodium hydroxide to the thick paste obtained in step (4) to adjust the pH to 11, fully stir for 1 h, filter, then add acetic acid to the filtrate to adjust the pH to 4.6, filter to obtain an insolu...
Embodiment 3
[0095] The preparation of embodiment 3 cannabinoids
[0096] The experimental steps are as follows:
[0097] (1) Grinding the raw material of industrial hemp mosaic leaves into 50-mesh coarse powder, baking at 60°C for 20 minutes, and the moisture content is 5.3%;
[0098] (2) soak the medicinal material obtained in step (1) with 8 times 30% ethanol at room temperature for 2 hours, extract twice, and combine to obtain the extract;
[0099](3) Concentrate the extract obtained in step (2) at 65°C to a paste concentrate (relative density 1.08, measured at 50°C);
[0100] (4) Extract the paste-like concentrated solution obtained in step (3) with 2 times the amount of medicinal material with n-hexane and extract twice, stir for 2 hours, take the upper layer after layering, combine the upper layer, and concentrate at 65°C to a thick paste (relative density 1.08, measured at 50°C);
[0101] (5) Add calcium hydroxide to the thick paste obtained in step (4) to adjust the pH to 11, f...
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