Dental implant surface coating and preparation method thereof
A surface coating and dental implant technology, applied in the field of medical material manufacturing, can solve the problems of reduced effectiveness, instability, degeneration, etc., and achieve excellent biocompatibility and bone fusion, and ensure the effect of mechanical strength.
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Embodiment 1
[0045] A method for preparing a dental implant surface coating, comprising the following steps:
[0046] (1) Digest the freeze-dried decellularized soft tissue with 0.1 M hydrochloric acid solution containing 1 mg pepsin for 24 hours to obtain a solution containing the decellularized matrix, and adjust the pH of the solution to 7 until it becomes a hydrogel;
[0047](2) Add hydroxyapatite particles in the range of 10-500 microns to the hydrogel obtained in step (1) to obtain a composite mixture, wherein the composite mixture comprises 5%wt% of acellular matrix and 95wt% of Hydroxyapatite;
[0048] (3) Apply the composite mixture obtained in step (2) to the surface of the roughened implant, and finally dry and sterilize.
Embodiment 2
[0050] A method for preparing a dental implant surface coating, comprising the following steps:
[0051] (1) Digest the freeze-dried decellularized soft tissue with 0.5M hydrochloric acid solution containing 5 mg of pepsin for 48 hours to obtain a solution containing the decellularized matrix, and adjust the pH of the solution to 9 until it becomes a hydrogel;
[0052] (2) Add hydroxyapatite particles in the range of 10-500 microns to the hydrogel obtained in step (1) to obtain a composite mixture, wherein the composite mixture comprises 20wt% acellular matrix and 80wt% hydroxyphosphorus gray stone;
[0053] (3) Apply the composite mixture obtained in step (2) to the surface of the roughened implant, and finally dry and sterilize.
Embodiment 3
[0055] A method for preparing a dental implant surface coating, comprising the following steps:
[0056] (1) Spray coating on the implant surface after roughening treatment contains 40wt% TiO 2 and a bottom layer of 60 wt% hydroxyapatite;
[0057] (2) Digest the freeze-dried decellularized soft tissue with 0.3M hydrochloric acid solution containing 3 mg of pepsin for 36 hours to obtain a solution containing the decellularized matrix, and adjust the pH of the solution to 7 until it becomes a hydrogel;
[0058] (3) Add hydroxyapatite particles in the range of 10-500 microns to the hydrogel obtained in step (2) to obtain a composite mixture, wherein the composite mixture comprises 15wt% acellular matrix and 85wt% hydroxyphosphorus gray stone;
[0059] (4) Apply the composite mixture obtained in step (3) to the surface of the bottom layer obtained in step (1), and finally dry and sterilize.
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