Technology for extracting naringin and polysaccharides in grapefruit skin by ultrasonic assisted double aqueous phases
A pomelo peel, two-water-phase technology is applied in the directions of sugar derivatives, sugar derivatives, sugar derivatives preparation, etc., and achieves the effects of simple operation process, improved efficiency and high efficiency
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Embodiment 1
[0054] An ultrasonic-assisted two-phase aqueous extraction process for naringin and polysaccharides in pomelo peels, comprising the following steps:
[0055] Step 1: Selection of pomelo peels: Choose fresh, non-rotten grapefruit peels, wash and set aside.
[0056] Step 2: drying: drying the pomelo peel until the moisture content is ≦0.5%.
[0057] Step 3: Crush and sieve: crush the pomelo peel with a high-speed universal grinder, and pass through a 80-100 mesh sieve for later use.
[0058] Step 4: Ultrasonic-assisted aqueous two-phase extraction: according to the ratio of material (pomelo peel powder): liquid (two-water phase) = 1:25-30, add pomelo peel powder to the two-phase system, and at the same time use ultrasonic waves for extraction .
[0059] Step 5: Suction filtration: After the extraction is completed, the extract is subjected to suction filtration.
[0060] Step 6: liquid separation: statically layer the suction filtrate, the upper liquid is the naringin extract...
Embodiment 2
[0076] An ultrasonic-assisted two-phase aqueous extraction process for naringin and polysaccharides in pomelo peels, comprising the following steps:
[0077] Step 1: Selection of pomelo peels: Choose fresh, non-rotten grapefruit peels, wash and set aside.
[0078] Step 2: drying: drying the pomelo peel until the moisture content is ≦0.5%.
[0079] Step 3: Crush and sieve: crush the pomelo peel with a high-speed universal grinder, and pass through a 80-100 mesh sieve for later use.
[0080] Step 4: Ultrasonic-assisted aqueous two-phase extraction: according to the ratio of material (pomelo peel powder): liquid (two-water phase) = 1:25-30, add pomelo peel powder to the two-phase system, and at the same time use ultrasonic waves for extraction .
[0081] Step 5: Suction filtration: After the extraction is completed, the extract is subjected to suction filtration.
[0082] Step 6: liquid separation: statically layer the suction filtrate, the upper liquid is the naringin extract...
Embodiment 3
[0098] An ultrasonic-assisted two-phase aqueous extraction process for naringin and polysaccharides in pomelo peels, comprising the following steps:
[0099] Step 1: Selection of pomelo peels: Choose fresh, non-rotten grapefruit peels, wash and set aside.
[0100] Step 2: drying: drying the pomelo peel until the moisture content is ≦0.5%.
[0101] Step 3: Crush and sieve: crush the pomelo peel with a high-speed universal grinder, and pass through a 80-100 mesh sieve for later use.
[0102] Step 4: Ultrasonic-assisted aqueous two-phase extraction: according to the ratio of material (pomelo peel powder): liquid (two-water phase) = 1:25-30, add pomelo peel powder to the two-phase system, and at the same time use ultrasonic waves for extraction .
[0103] Step 5: Suction filtration: After the extraction is completed, the extract is subjected to suction filtration.
[0104] Step 6: liquid separation: statically layer the suction filtrate, the upper liquid is the naringin extract...
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