Preparation method and application of nano MoS2-loaded carbon material compound

A technology of carbon materials and composites, which is applied in the field of preparation of carbon material-loaded nano-MoS2 composites, can solve the problems of cumbersome steps for carbon material-loaded nano-MoS2, and achieve excellent anti-friction and anti-wear properties

Inactive Publication Date: 2019-07-23
LANZHOU INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The object of the present invention is to provide carbon material loaded nano-MoS 2 The preparation method and application of

Method used

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  • Preparation method and application of nano MoS2-loaded carbon material compound
  • Preparation method and application of nano MoS2-loaded carbon material compound
  • Preparation method and application of nano MoS2-loaded carbon material compound

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[0019] A carbon material loaded with nano-MoS 2 The preparation method of the composite, the steps are as follows,

[0020] Add a certain amount of ammonium tetrathiomolybdate and carbon nanomaterials to N,N-dimethylformamide, and after the mixture is uniformly dispersed by ultrasonic, add hydrazine hydrate and continue ultrasonic dispersion;

[0021] The mixture obtained by ultrasonic dispersion was transferred to a solvothermal reaction kettle with a Teflon lining tube, the reaction kettle was sealed, and the reaction kettle was heated to 200°C for a few hours, then cooled, placed in a centrifuge, and centrifuged at 9000 rpm. Wash with deionized water; the solid material obtained after centrifugation is vacuum-dried overnight at 50°C to obtain the product, which is the carbon material@MoS 2 .

[0022] Further, the mass ratio of the carbon material to the amine tetrathiomolybdate is 2.2:1, the mass volume ratio to DMF is 1:1 mg / mL, and the mass volume ratio to hydrazine hydrate is 1...

Example Embodiment

[0028] Example 1

[0029] A carbon material loaded with nano-MoS 2 The preparation method of the composite, the steps are as follows:

[0030] 27.5mg(NH 4 ) 2 MoS 4 And 12.5 mg of carbon nanotubes (CNTs) were added to 12.5 mL of DMF, the mixture was sonicated for 10 minutes and then 0.125 mL of hydrazine hydrate was added, and the ultrasonic dispersion was continued for 30 minutes. The mixture was then transferred to a 50 mL solvothermal reactor with a Teflon-lined tube. After sealing, heat to 200°C to react for 10 hours. The obtained reaction solution was placed in a centrifuge, centrifuged at 9000 rpm for 3 minutes, and washed with deionized water. The solid material after centrifugation and washing was dried overnight in a vacuum at 50°C, and the product obtained is the carbon nanotube loaded nano-MoS 2 Composite (CNTs@MoS 2 ).

[0031] Add 1.0wt% CNTs, 1.0wt% MoS to the polyether base oil 2 And 1.0wt%CNTs@MoS 2 , Test its tribological properties after the ultrasonic dispersion...

Example Embodiment

[0032] Example 2

[0033] A carbon material loaded with nano-MoS 2 The preparation method of the composite, the steps are as follows:

[0034] 27.5mg(NH 4 ) 2 MoS 4 And 12.5 mg of fullerene C60 were added to 12.5 mL of DMF, the mixture was sonicated for 10 minutes and then 0.125 mL of hydrazine hydrate was added, and the ultrasonic dispersion was continued for 30 minutes. The mixture was then transferred to a 50 mL solvothermal reactor with a Teflon-lined tube. After sealing, heat to 200°C to react for 10 hours. The obtained reaction solution was placed in a centrifuge, centrifuged at 9000 rpm for 3 minutes, and washed with deionized water. The solid material after centrifugation and washing was dried overnight in vacuum at 50°C, and the product obtained is fullerene C60 loaded nano-MoS 2 Complex (C60@MoS 2 ).

[0035] Add 1.0wt% C60, 1.0wt% MoS to polyether base oil 2 And 1.0wt% C60@MoS 2 , Test its tribological properties after the ultrasonic dispersion is uniform.

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Abstract

The invention discloses a preparation method and application of a nano MoS2-loaded carbon material compound. A carbon material is prepared from graphene, a carbon nanotube, fullerene C60 and fullereneC70. The nano MoS2-loaded carbon material compound prepared by the preparation method disclosed by the invention can form a stable dispersion system in synthetic lubricating oil, and shows excellentantiwear and friction reducing performance within a range of 50 to 125 DEG C.

Description

technical field [0001] The invention relates to a carbon material loaded nano-MoS 2 The preparation method and application of the compound. Background technique [0002] With the rapid development of science and technology, modern industrial equipment is faced with more severe service conditions, such as high speed, heavy load and high temperature, all of which will lead to an increase in the surface temperature of the friction pair. In the current lubricant service environment, there are many actual working conditions with temperatures higher than 200°C or 300°C. For example, for the next generation of high-temperature-resistant aircraft engine oil, it is expected to be able to adapt to the working temperature of 260-427°C. Many equipment in the metallurgical industry need to work Lubricating grease with a temperature as high as 200-300°C. In order to meet the lubrication requirements under high temperature and severe working conditions, many synthetic base oils, such as ...

Claims

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Application Information

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IPC IPC(8): C10M125/06
CPCC10M125/06C10M2201/041C10M2201/043
Inventor 王晓波吴新虎宫奎亮
Owner LANZHOU INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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