Low-temperature used blend oil with balanced omega-6 and omega-3 unsaturated fatty acids and preparation method thereof
A technology of unsaturated fatty acids and blended oils, which is applied in the direction of fat oil/fat refining, fat production, edible oil/fat, etc., and can solve the problems of not considering high temperature resistance, lack of reasonable ratio of fatty acids, and not considering the intake of non-cooking oil fatty acids and other issues, to achieve the effect of safe source, extended storage period and easy acceptance
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Embodiment 1
[0049] (1) Preparation of debittered linseed oil:
[0050] a. Winterize linseed crude oil at 8°C for 15 hours, and filter to obtain filtered oil; b. Heat the above-mentioned filtered linseed oil to 30°C, under a pressure of 0.08MPa, use 500nm tangential flow inorganic ceramic membrane for membrane separation to obtain membrane-permeable oil; c. Use membrane-permeable oil as mobile phase and chromatographic packing as stationary phase for chromatographic separation. The chromatographic packing is made of food-grade beer silica gel with a particle size of 200 mesh, the elution volume is 15 times the volume of the packed beer silica gel filler, and the outflowing oil is received in a container; d. The above-mentioned received oil is heated to 35°C, and under a pressure of 0.2MPa, a cut-off filter with a pore size of 100nm is used. The flow inorganic ceramic membrane is used for membrane separation again to obtain the permeable oil liquid, which is the desired debittered linseed o...
Embodiment 2
[0054] (1) Preparation of debittered linseed oil:
[0055]a. Winterize linseed crude oil at 10°C for 24 hours, filter to obtain the filtered oil; b. heat the above-mentioned filtered oil to 50°C, and use a cut-off filter with a pore size of 1000nm under a pressure of 0.05MPa. Purify by flowing inorganic ceramic membrane to obtain membrane-permeable oil; c. Use membrane-permeable oil as the mobile phase and chromatographic packing as the stationary phase for chromatographic separation. The chromatographic packing is made of food-grade beer silica gel with a particle size of 800 mesh. The volume is 20 times the volume of the installed beer silica gel filler, and the outflowing oil is received in a container; d. Heat the above-mentioned received oil to 60°C, and use a tangential flow inorganic ceramic membrane with a pore size of 50nm under a pressure of 0.1MPa Further purification to obtain the membrane-permeable oil, which is the desired debittered linseed oil;
[0056] (2) Pr...
Embodiment 3
[0059] (1) Preparation of debittered linseed oil:
[0060] a. Winterize linseed crude oil at -1°C for 5 hours, filter to obtain filtered oil; b. Heat the above-mentioned filtered linseed oil to 20°C, under a pressure of 0.15MPa, use a pore diameter Purified by a 600nm tangential flow inorganic ceramic membrane to obtain a membrane-permeable oil; c. Use the membrane-permeable oil as the mobile phase and the chromatographic packing as the stationary phase for chromatographic separation. The chromatographic packing is made of food-grade beer silica gel with a particle size of 300 The elution volume is 16 times the volume of the packed beer silica gel filler, and the outflowing oil is received in a container; d. Heat the above-mentioned received oil to 50°C, and use a tangential filter with a pore size of 100nm under a pressure of 0.2MPa. The flow of inorganic ceramic membrane is further purified to obtain the membrane-permeable oil, which is the desired debittered linseed oil;
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