Preparation method of two-dimensional layered glycerin oxidation nano-catalyst
A nano-catalyst, two-dimensional layered technology, applied in the direction of catalyst activation/preparation, preparation of organic compounds, physical/chemical process catalysts, etc., can solve the problems of complex reaction process and poor catalytic effect, and achieve novel structure , the effect of good product selectivity
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[0014] Embodiment 1 utilizes oxidation method to prepare graphene oxide.
[0015] Combining graphene oxide and mesoporous silicon to construct a two-dimensional layered graphene-mesoporous silicon precursor.
[0016] 0.5 g of cerium nitrate was dissolved in 3 mL of ethanol solution, and then mixed with 0.2 g of graphene-mesoporous silicon composite, and dried and calcined to prepare cerium oxide and graphene-mesoporous silicon composite.
[0017] The prepared cerium oxide, graphene-mesoporous silicon composite material and strong alkali solution are mixed and heated, and after a series of basic treatment processes such as washing, filtering and drying, a graphene-supported two-dimensional ordered layered Ceria support.
[0018] Mix 0.2 g of graphene-supported two-dimensional ordered layered ceria carrier with 1.2 mL of 1 g / 100 mL chloroauric acid and 2.25 mL of 1 g / 100 mL polyvinyl alcohol, and finally add 4.5 mL of 0.38 g / 100 mL sodium borohydride and stirred for 90 minute...
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