Perfume used for refreshing pungent type flavor cigarettes, preparation method thereof, and applications of perfume in cigarettes
A technology for flavoring and clearing spices for tobacco is applied in the field of tobacco processing, which can solve problems such as loss of aroma, and achieve the effects of improving internal quality, simple process and obvious effect.
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Embodiment 1
[0030] The invention discloses a spice for tobacco with a clear and spicy flavor, which is prepared from the following raw materials in parts by weight: 10 g of prickly ash buds, 20 g of perilla, and 20 g of Pangpengxiang. The preparation method of the compound natural plant extract comprises the following steps:
[0031] (1) Pretreatment: Pick fresh pepper bud leaves, perilla leaves and Pangpengxiang leaves, wash them with water, drain them, put them in an oven, and dry them at 60°C. Dry the leaves of the three plants After grinding and crushing, pass through a 60-mesh sieve;
[0032] (2) Distillation and extraction: Mix pepper buds, perilla leaves, and Pangpengxiang powder, take Zanthoxylum bungeanum, perilla, and Pengpengxiang mixed powder, add 1000 mL of distilled water, heat in a water bath at 55°C for 4 hours, and use 30 mL of ether solvent in Extract aroma substances in a water bath environment at 60°C to obtain a primary feed liquid;
[0033] (3) Concentration and pu...
Embodiment 2
[0035] The invention discloses a spice with clear and spicy fragrance, which is prepared from the following raw materials in parts by weight: 12.5 g of prickly ash buds, 25 g of perilla, and 12.5 g of Pengpengxiang. The preparation method of the clear and pungent type tobacco spices comprises the following steps:
[0036] (1) The pretreatment steps are the same as in Example 1;
[0037] (2) Distillation and extraction: Take the mixed powder of pepper buds, perilla and Pangpengxiang, add 1000 mL of distilled water, heat in a water bath at 65°C for 3.5 hours, use 40 mL of ether solvent to extract aroma substances in a water bath at 60°C, and obtain a primary feed solution ;
[0038] (3) Concentration and purification: add 20 g of anhydrous sodium sulfate to the primary feed liquid extracted in step (2), dry for 7 h, take the supernatant to obtain a secondary feed liquid; put the secondary feed liquid in a water bath at a temperature of Rotary evaporation was carried out at 48°...
Embodiment 3
[0040] The invention discloses a spice for tobacco with clear and spicy flavor, which is made of the following raw materials in parts by weight: 15 g of prickly ash buds, 20 g of perilla, and 15 g of Pangpengxiang. The preparation method of the clear and pungent type tobacco spices comprises the following steps:
[0041] (1) The pretreatment steps are the same as in Example 1;
[0042] (2) Distillation and extraction: Take the mixed powder of pepper buds, perilla and Pangpengxiang, add 1000 mL of distilled water, heat in a water bath at 60°C for 5 hours, use 40 mL of ether solvent to extract aroma substances in a water bath at 60°C, and obtain a primary feed solution ;
[0043] (3) Concentration and purification: Add about 30 g of anhydrous sodium sulfate to the primary feed liquid extracted in step (2), dry for 7.5 h, take the supernatant to obtain the secondary feed liquid; put the secondary feed liquid in the water bath temperature Under the condition of below 47°C, carry...
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