Diamond gradient coating and preparation method and application thereof

A gradient coating and diamond technology, applied in metal material coating process, coating, gaseous chemical plating, etc., can solve the problems of easy wear, unstable water collection materials, and difficulty in directional water collection, and achieve good collection Effect of water efficiency, good mechanical wear resistance and chemical stability

Active Publication Date: 2020-01-14
SHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to provide a diamond gradient coating and its preparation method and application, aiming to solve the technical problems that the existing water-collecting materials are unstable, easy to wear, and difficult to achieve directional water collection

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  • Diamond gradient coating and preparation method and application thereof
  • Diamond gradient coating and preparation method and application thereof
  • Diamond gradient coating and preparation method and application thereof

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preparation example Construction

[0020] On the one hand, the embodiment of the present invention provides a kind of preparation method of diamond gradient coating, and this preparation method comprises the following steps:

[0021] S01: providing a substrate, and performing a hydrophilic treatment on the surface of the substrate;

[0022] S02: placing the hydrophilic treated substrate in a nanodiamond suspension, and performing crystal planting treatment;

[0023] S03: Depositing and growing diamond on the surface of the substrate after the crystal planting treatment, so that the concentration of nano-diamond particles and the particle size of nano-diamond particles along the direction away from the surface of the substrate are gradually increased to obtain a diamond gradient coating.

[0024] In the preparation method of the diamond gradient coating provided by the embodiment of the present invention, the surface of the substrate is firstly subjected to hydrophilic treatment to form a hydrophilic substrate s...

Embodiment 1

[0049] A kind of preparation method of diamond gradient coating, concrete operation steps are as follows:

[0050] Step 1: cleaning the surface of the titanium sheet substrate. First, use deionized water to ultrasonically clean twice, each time for 5 minutes, and finally use alcohol to ultrasonically clean for 5 minutes, and blow dry with nitrogen.

[0051] Step 2: corroding the cleaned titanium sheet to form titanium oxide and negatively charge the surface. The corrosion treatment is: ultrasonic cleaning in alkaline solution for 8 minutes, and then cleaning in deionized water for 2 minutes, wherein the alkaline solution is a mixed solution with a volume ratio of ammonia water: hydrogen peroxide: deionized water = 1:1:5.

[0052] Step 3: treating the corroded substrate with oxygen plasma to make the surface into a super-hydrophilic surface.

[0053] Step 4: Clean the super-hydrophilic surface of the substrate, and clean the solution remaining in the sheet. Use deionized wat...

Embodiment 2

[0057] A kind of preparation method of diamond gradient coating, concrete operation steps are as follows:

[0058] Step 1: Clean the surface of the silicon wafer, first use deionized water to ultrasonically clean twice, each time for 5 minutes, and finally use alcohol to ultrasonically clean for 5 minutes, and blow dry with nitrogen.

[0059] Step 2: Etching the cleaned silicon wafer to form silicon oxide and negatively charge the surface. The corrosion treatment is: ultrasonic cleaning in alkaline solution for 8 minutes, and then cleaning in deionized water for 2 minutes. The alkaline solution is a mixed solution with a volume ratio of ammonia water: hydrogen peroxide: deionized water = 1:1:5.

[0060] Step 3: Treat the corroded substrate in a mixture of concentrated sulfuric acid and potassium nitrate to make the surface super-hydrophilic.

[0061] Step 4: cleaning the super-hydrophilic treated substrate, and cleaning the etching solution remaining in the silicon wafer. U...

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Abstract

The invention belongs to the technical field of water collecting materials, in particular to a diamond gradient coating and a preparation method and an application thereof. The preparation method of the diamond gradient coating comprises the following steps: providing a matrix and carrying out hydrophilic treatment on the surface of the matrix; placing the matrix after hydrophilic treatment in a nano diamond suspension for crystal implantation; and depositing and growing diamond on the surface of the matrix after crystal implantation, wherein the nano diamond particle concentrations and nano diamond particle grain sizes along the direction deviated from the surface of the matrix are increased to obtain the diamond gradient coating. According to the preparation method, a wettability gradient of the diamond gradient coating from being super-hydrophobic to being super-hydrophilic can be achieved, and the obtained diamond gradient coating has very good mechanical wear resistance and chemical stability, so that the diamond gradient coating for directional water collection has a very good water collecting efficiency.

Description

technical field [0001] The invention belongs to the technical field of water-collecting materials, and in particular relates to a diamond gradient coating and a preparation method and application thereof. Background technique [0002] Water harvesting by heterogeneous condensation and fog collection is of great importance in daily life and industrial applications, and the unique combination of surface morphology and wettability exhibited by natural and biological species is receiving increasing attention from the scientific community. The surface morphologies of these species exhibit unique micro- and nanostructural arrangements that play crucial roles in water vapor condensation and fog collection. Since the 20th century, water capture technologies have received increasing attention due to more severe water scarcity problems worldwide, especially those in inhabited deserts and arid regions. Rainfall is scarce in these areas, and some plants and animals rely on fog and mois...

Claims

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Application Information

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Patent Type & AuthorityApplications(China)
IPC IPC(8): C23C16/27C23C16/02
CPCC23C16/271C23C16/0272C23C16/0227
Inventor唐永炳王星永王陶
OwnerSHENZHEN INST OF ADVANCED TECH CHINESE ACAD OF SCI