Aluminum-plated AlN nanofiber reinforced Al-Fe-based nanoporous alloy material and a preparation method thereof
A technology of nanofibers and alloy materials, applied in the field of composite materials, which can solve the problems of heavy weight, high cost, and high energy consumption
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Embodiment 1
[0030] 1. Preparation of Al-Fe-based alloy nanopowder
[0031] Using α-Al with an average particle size of 5 μm 2 o 3 The powder is a source of nano-Al powder, treated by ball milling, the mill speed is 92r / min, the mass ratio of ball to material is 15:1, protected by argon, and the ball milling time is 5h; the powder after ball milling is reduced in hydrogen at 180°C to obtain Nano-Al powder with an average particle size of 12nm;
[0032] Using Fe powder with an average particle size of 10 μm as the source of nano-Fe powder, ball milling, the mill speed is 500r / min, the mass ratio of ball to material is 25:1, protected by argon, and the ball milling time is 8h; get 10nm nano-Fe powder body;
[0033] 2. Pretreatment of AlN nanofibers
[0034] AlN nanofibers with an average diameter of 8nm and an average length of 90nm are used as reinforcing components; the AlN nanofibers are activated with a sodium hydroxide solution with a concentration of 0.1mol / L, the treatment tempera...
Embodiment 2
[0046] 1. Preparation of Al-Fe-based alloy nanopowder
[0047] Using α-Al with an average particle size of 5 μm 2 o 3The powder is a nano-Al powder source, ball milled, the mill speed is 92r / min, the mass ratio of the ball to material is 15:1, the argon gas is protected, and the ball milling time is 4.5h; the powder after ball milling is reduced in hydrogen at 180°C, A nano-Al powder with an average particle size of 28nm was obtained;
[0048] Using Fe powder with an average particle size of 10 μm as the source of nano-Fe powder, ball milling, the mill speed is 500r / min, the mass ratio of ball to material is 25:1, protected by argon, and the ball milling time is 5h; 17nm nano-Fe powder is obtained body;
[0049] 2. Pretreatment of AlN nanofibers
[0050] AlN nanofibers with an average diameter of 12nm and an average length of 155nm are used as reinforcing components; the AlN nanofibers are activated with a sodium hydroxide solution with a concentration of 0.1mol / L, the tre...
Embodiment 3
[0062] 1. Preparation of Al-Fe-based alloy nanopowder
[0063] Using α-Al with an average particle size of 5 μm 2 o 3 The powder is a source of nano-Al powder, treated by ball milling, the mill speed is 92r / min, the mass ratio of ball to material is 15:1, protected by argon, and the ball milling time is 3.5h; the powder after ball milling is reduced in hydrogen at 180°C. Obtain nano-Al powder with an average particle size of 16nm;
[0064] Using Fe powder with an average particle size of 10 μm as the source of nano-Fe powder, ball milling, the mill speed is 500r / min, the mass ratio of ball to material is 25:1, protected by argon, and the ball milling time is 6h; get 13nm nano-Fe powder body;
[0065] 2. Pretreatment of AlN nanofibers
[0066] AlN nanofibers with an average diameter of 9nm and an average length of 115nm are used as reinforcing components; the AlN nanofibers are activated with a sodium hydroxide solution with a concentration of 0.1mol / L, the treatment temper...
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