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A kind of preparation method of interlayer toughened composite material

A technology for toughening composite materials and composite material layers, applied in the field of composite material science, can solve the problems of inability to carry out large-scale promotion and use, increase the structural weight and manufacturing cost, increase the viscosity of the matrix resin, etc. Toughness effect, low cost, the effect of enhancing its own interlayer toughness

Active Publication Date: 2021-11-23
JIANGSU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Matrix toughening refers to adding rubber or thermoplastic materials to the resin to improve the fracture toughness of the composite material, but this method will increase the weight of the structure and manufacturing costs, and the addition of thermoplastic resin increases the viscosity of the matrix resin, resulting in the composite material. In-plane performance degradation
Nanostructure toughening methods mainly include inserting carbon nanotube tulle between layers or constructing a combined structure of fibers and carbon nanotubes to achieve the effect of material toughening, but these technologies are relatively complicated and are still in the basic research stage. There are many problems in the process, and it is impossible to carry out large-scale promotion and use

Method used

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  • A kind of preparation method of interlayer toughened composite material
  • A kind of preparation method of interlayer toughened composite material
  • A kind of preparation method of interlayer toughened composite material

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Embodiment

[0032] An interlayer toughened composite material board containing agglomerated microcapsules in this embodiment includes fiber prepreg stacks and epoxy resin glue, the epoxy resin glue contains microcapsules, and the resin glue is filled and coated on the surface of the cured prepreg stack. In this embodiment, 10 layers of fiber prepreg with a thickness of 0.15 mm are laid in one direction to form a stack with a thickness of 1.5 mm, and the finally formed interlayer toughened sample is a composite plate structure with a thickness of 3 mm.

[0033] figure 2 It is a schematic diagram of the distribution of microcapsules in the resin matrix. from figure 2 It can be seen that the capsules are distributed in the interlayer resin matrix in the form of agglomeration. During the curing process of placing the sample on a hot press at a high temperature of 120°C and a high pressure of 4Mpa, the capsules are squeezed and ruptured, which induces a polymerization reaction in the capsu...

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Abstract

The invention discloses a preparation method of an interlayer toughened composite material. The steps are as follows: step 1: selecting microcapsules with multi-capsule cores as the interlayer toughened material of the composite material, and step 2: impregnating continuous fibers in a resin matrix , to make a prepreg of resin matrix and fiber; Step 3: Lay the prepreg described in Step 2 along a single direction, and transfer it to a hot press to heat and press for curing treatment; Step 4: Put the microcapsules, ring Oxygen resin and curing agent are mixed, and the resin glue with microcapsules is made after manual stirring; Step 5: Use a brush to apply the resin glue with microcapsules on the surface of the cured prepreg stack; Step 6: Put the two The prepreg stacks that have been coated and cured in Step 5 are laminated, and then transferred to a hot press for heating and pressing for interlayer matrix curing. The microcapsules used in the preparation method of the present invention have cheap raw materials, mature preparation technology, low cost and high operability, and can be popularized in large-scale industrialization.

Description

technical field [0001] The invention belongs to the process preparation technology of carbon fiber / resin-based composite materials, specifically a composite material modification method using agglomerated microcapsules as toughening materials, and belongs to the field of composite material science and technology. Background technique [0002] Composite materials have unique advantages such as high specific strength, high specific stiffness, heat resistance, corrosion resistance, and good designability. At present, they are widely used in the design and manufacturing of high-speed trains, aerospace, wind turbines, and automobiles. For example, large passenger aircraft Boeing The amount of composite materials on the 787 is as high as 50%, and the amount of composite materials on the fan blades of wind turbines exceeds 90%. [0003] As one of the commonly used components, composite panels are a typical layered structure, mainly relying on thermosetting matrix resin for bonding,...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B32B9/00B32B9/04B32B3/08B32B7/12B32B27/04B32B37/06B32B37/10B32B37/12C08L63/00C08L61/24C08G59/66C08G59/24
CPCB32B3/08B32B3/085B32B5/02B32B5/26B32B7/12B32B37/06B32B37/10B32B37/1284B32B2250/20B32B2262/106B32B2307/558B32B2603/00B32B2605/08B32B2605/10B32B2605/18C08G59/245C08G59/66C08L63/00C08L2205/025C08L61/24
Inventor 郝文峰王奔王定川赵国旗骆英陈浩森方岱宁
Owner JIANGSU UNIV
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