Preparation method of potassium chloropalladate
A technology of potassium chloropalladate and palladium chloride, applied in chemical instruments and methods, ruthenium/rhodium/palladium/osmium/iridium/platinum compounds, inorganic chemistry, etc. Complicated operations, etc.
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0036] Take 100mL PdCl 2 Put the solution in a beaker, add 50mL HClO after heating up to 60°C 4 , stirred for 45min. The temperature of the Pd-containing solution was raised to 100°C, and 300 mL of saturated KCl solution was added to the system, and stirred for 60 min. The resulting solution was cooled in ice water and dried in a vacuum oven at 50°C. Testing, storage.
[0037] result:
[0038] Potassium chloropalladate synthesis rate: 95%;
[0039] Potassium chloropalladate purity: 99.5%;
Embodiment 2
[0041] Take 100mL PdCl 2 Put the solution in a beaker, add 60mL HClO after heating up to 80°C 4 , stirred for 60min. The temperature of the Pd-containing solution was raised to 140°C, and 500 mL of saturated KCl solution was added to the system, and stirred for 60 min. The resulting solution was cooled in ice water and dried in a vacuum oven at 50°C. Testing, storage.
[0042] result:
[0043] Potassium chloropalladate synthesis rate: 95.2%;
[0044] Potassium chloropalladate purity: 99.6%;
Embodiment 3
[0046] Take 100mL PdCl 2 Place the solution in a beaker, add 30mL HClO after heating up to 70°C 4 , stirred for 50min. The temperature of the Pd-containing solution was raised to 120°C, and 400 mL of saturated KCl solution was added to the system, and stirred for 50 min. The resulting solution was cooled in ice water and dried in a vacuum oven at 50°C. Testing, storage.
[0047] result:
[0048] Potassium chloropalladate synthesis rate: 95.4%;
[0049] Potassium chloropalladate purity: 99.6%;
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More