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Method for measuring and calculating relationship between vacuum degree of low-temperature gas cylinder and daily evaporation rate and adsorption capacity

A technology of vacuum degree and evaporation rate, which is applied in the field of measuring the relationship between the vacuum degree of low-temperature gas cylinders and the daily evaporation rate and adsorption capacity, and can solve the problems of difficulty in evaluating the vacuum life period of the interlayer of low-temperature gas cylinders.

Active Publication Date: 2020-03-24
ZHANGJIAGANG FURUI SPECIAL EQUIP CO LTD
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Problems solved by technology

[0004] Now due to the lack of air leakage or the relationship between the vacuum degree of the interlayer of the cryogenic gas cylinder and the adsorption capacity after the material is deflated, and the relationship between the vacuum degree of the interlayer and the static daily evaporation rate, the vacuum life of the interlayer of the cryogenic gas cylinder after the air leakage or the material is deflated Duration is difficult to assess

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  • Method for measuring and calculating relationship between vacuum degree of low-temperature gas cylinder and daily evaporation rate and adsorption capacity
  • Method for measuring and calculating relationship between vacuum degree of low-temperature gas cylinder and daily evaporation rate and adsorption capacity
  • Method for measuring and calculating relationship between vacuum degree of low-temperature gas cylinder and daily evaporation rate and adsorption capacity

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Embodiment Construction

[0020]The present invention will be further described in detail below in conjunction with specific embodiments and accompanying drawings.

[0021] The calculation method of the relationship between the vacuum degree of the cryogenic gas cylinder, the daily evaporation rate and the adsorption capacity, the steps of the method are as follows:

[0022] (1) Prepare the measuring device, such as figure 1 As shown, the measuring device includes: mass flow meter 1, vacuum measuring pipe 2, vacuum gauge 3, burette 52, vacuum fine-tuning valve 51, silicone oil 5, vacuum valve 6, evacuation valve 71, air source valve 81, air source 8, vacuum Unit 7; in the present embodiment, the accuracy of the mass flowmeter 1 is not less than 1%; the vacuum gauge 3 has a range of 10 5 Pa~10 -5 The composite vacuum gauge of Pa has an accuracy of not less than 15%. Silicone oil 5 is diffusion pump silicone oil available on the market. Quantitative gas brings influence; One port of vacuum measuring p...

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Abstract

The invention discloses a method for measuring and calculating the relationship between the vacuum degree of a low-temperature gas cylinder and the daily evaporation rate and the adsorption capacity.The method comprises the following steps: (1) preparing a measuring device; (2) measuring and calculating the basic values of the background interlayer vacuum degree and the static daily evaporation rate of the low-temperature gas cylinder into which the low-temperature liquid is injected; (3) filling the interlayer of the low-temperature gas cylinder with trace gas for multiple times to reduce the vacuum degree of the interlayer of the low-temperature gas cylinder, and measuring and calculating the vacuum degree, the static daily evaporation rate and the adsorption capacity of the interlayerof the low-temperature gas cylinder after the gas is filled each time; (4) drawing a change relation curve of the interlayer vacuum degree and the static daily evaporation rate according to the recorded interlayer vacuum degree and the static daily evaporation rate; and drawing an actual adsorption isotherm according to the recorded interlayer vacuum degree after each time of inflation and the corresponding adsorption capacity. According to the measuring and calculating method, the change relation between the vacuum degree of the interlayer of the low-temperature gas cylinder after gas leakageand deflation and the static daily evaporation rate and the adsorption capacity can be measured and calculated, and the change relation can be shown through a drawn curve.

Description

technical field [0001] The invention relates to the field of low-temperature gas cylinders for storing low-temperature liquids, in particular to a method for measuring and calculating the relationship between the vacuum degree of low-temperature gas cylinders, daily evaporation rate and adsorption capacity. Background technique [0002] A cryogenic gas cylinder is a vacuum insulated container for storing and transporting cryogenic liquids, such as liquid hydrogen, liquid nitrogen, liquid oxygen, liquid argon, and liquefied natural gas. The cryogenic gas cylinder has an outer cylinder and an inner cylinder located in the outer cylinder. The cylinder, the interlayer between the inner and outer cylinders is a vacuum insulation layer, and an adsorbent for absorbing gas is placed in the interlayer to maintain the vacuum; the vacuum degree of the cryogenic gas cylinder refers to the vacuum degree of the interlayer of the cryogenic gas cylinder. The service life of the bottle is cl...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01M13/00G01D21/02G01L21/00
CPCG01D21/02G01L21/00G01M13/00
Inventor 何晓冬黄强华陈光奇朱鸣李晓峰朱关标
Owner ZHANGJIAGANG FURUI SPECIAL EQUIP CO LTD
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